GREEN APPROACH FOR THE PREPARATION OF 2-ARYL-1, 3-BENZOXAZOLE DERIVATIVES BY USING Amla Fruit EXTRACT

IF 0.5 Q4 EDUCATION & EDUCATIONAL RESEARCH Rasayan Journal of Chemistry Pub Date : 2023-01-01 DOI:10.31788/rjc.2023.1628174
Shahabaj M. Bagwan, M. Farooqui, M. A. Pathan, Satish M Patil, Mohamad Asif
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Abstract

One pot, rapid and green preparation of 2-aryl-1,3-benzoxazole and their derivatives via the reaction of o-amino phenol and substituted aryl aldehydes by using amla fruit extract at room temperature or under microwave radiation. Amla fruit extract is a biocatalyst associated with low-cost, inexpensive, non-volatile, and environmentally friendly. The prepared catalyst shows many chemical, phytochemical, and anti-oxidant constituents, which are unfavorable to increase the acidic contents of water extract. The noteworthy benefits of this process are simple, easy methodology, an excellent yield of product, minimum time of reaction, ease of separation, easy work, and green catalyst. The prepared compound where characterized by analytical or spectroscopic techniques such as FT-IR (infrared) spectrum, H1-NMR, C13-NMR, and LC-MS (Mass) analysis.
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摘要以阿姆拉果提取物为原料制备2-芳基- 1,3 -苯并恶唑衍生物的绿色方法
以阿姆拉果提取物为原料,在室温或微波辐射下,以邻氨基酚和取代芳基醛为原料,一锅、快速、绿色制备2-芳基-1,3-苯并恶唑及其衍生物。阿姆拉果提取物是一种低成本、廉价、不挥发、环保的生物催化剂。所制备的催化剂含有多种化学、植物化学和抗氧化成分,不利于提高水提物的酸性含量。该工艺具有方法简单、收率高、反应时间短、易分离、操作简便、催化剂环保等优点。用FT-IR(红外)光谱、H1-NMR、C13-NMR和LC-MS(质量)分析等分析或光谱技术对所制备的化合物进行表征。
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来源期刊
Rasayan Journal of Chemistry
Rasayan Journal of Chemistry Energy-Energy (all)
CiteScore
1.90
自引率
0.00%
发文量
196
期刊介绍: RASĀYAN Journal of Chemistry [RJC] signifies a confluence of diverse streams of chemistry to stir up the cerebral powers of its contributors and readers. By introducing the journal by this name, we humbly intent to provide an open platform to all researchers, academicians and readers to showcase their ideas and research findings among the people of their own fraternity and to share their vast repository of knowledge and information. The journal seeks to embody the spirit of enquiry and innovation to augment the richness of existing chemistry literature and theories. We also aim towards making this journal an unparalleled reservoir of information and in process aspire to inculcate and expand the research aptitude.
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