Saad Nadeem Saad Nadeem, Fahim Uddin Fahim Uddin, Maizatul Shima Shaharun Maizatul Shima Shaharun, Mohamed Ibrahim Abdul Mutalib Mohamed Ibrahim Abdul Mutalib
{"title":"Yield Optimization for One Pot Synthesis of Cu, Mn based Metalloporphyrin","authors":"Saad Nadeem Saad Nadeem, Fahim Uddin Fahim Uddin, Maizatul Shima Shaharun Maizatul Shima Shaharun, Mohamed Ibrahim Abdul Mutalib Mohamed Ibrahim Abdul Mutalib","doi":"10.52568/001119/jcsp/44.05.2022","DOIUrl":null,"url":null,"abstract":"Cu and Mn based tetraphenyl porphyrin namely CuTPP and MnTPP were synthesized through a one pot route with a modified procedure and the reaction conditions (Temperature and time) were optimized based on the energy consumption during the synthesis of the target macrocyclic ligands. The temperature (145oC and 160oC) and time (3, 4, 8 hr) were used to study the effect on the product yield. The optimized values obtained using MATLAB routines are 3.7 hr and 145oC.","PeriodicalId":17253,"journal":{"name":"Journal of the chemical society of pakistan","volume":"1 1","pages":""},"PeriodicalIF":0.6000,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of the chemical society of pakistan","FirstCategoryId":"92","ListUrlMain":"https://doi.org/10.52568/001119/jcsp/44.05.2022","RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CHEMISTRY, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 0
Abstract
Cu and Mn based tetraphenyl porphyrin namely CuTPP and MnTPP were synthesized through a one pot route with a modified procedure and the reaction conditions (Temperature and time) were optimized based on the energy consumption during the synthesis of the target macrocyclic ligands. The temperature (145oC and 160oC) and time (3, 4, 8 hr) were used to study the effect on the product yield. The optimized values obtained using MATLAB routines are 3.7 hr and 145oC.
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This journal covers different research areas in the field of Chemistry. These include; Analytical Chemistry, Applied Chemistry, Biochemistry, Environmental Chemistry, Industrial Chemistry, Inorganic Chemistry, Organic Chemistry and Physical Chemistry. The journal publishes full length articles and Reviews from researchers in academia in addition to featuring comments. Chemical Research presents short, concise and critical articles offering easy-to-read overviews of basic research and applications in all areas of chemistry.
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