Jing Huang Jing Huang, Jincan Lei Jincan Lei, Shixian Zhao and Yan Li Shixian Zhao and Yan Li
{"title":"A Fast Detection Method for Pesticide Residues by Spectrometry Technique","authors":"Jing Huang Jing Huang, Jincan Lei Jincan Lei, Shixian Zhao and Yan Li Shixian Zhao and Yan Li","doi":"10.52568/001189/jcsp/44.06.2022","DOIUrl":null,"url":null,"abstract":"In this paper, a fast detection method for pesticide residues was proposed, and the qualitative and quantitative detection of the pesticide could be got at once by the method of solution of multiple linear regression equations which were obtained by dual wavelength absorbance and fluorescence spectrometry with least squares method. Moreover, it could detect two kinds of mixed pesticides. Four selected pesticides, aldicarb, fenitrothion, fenvalerate, and chlorothalonil were detected by the method. The results shown that there were good linear relationship in the range of 0.01-1 ppm, and R2 > 0.90. And the method could 100% discriminate the four pesticide residues, the limit of detection was below 8 ppb both single one and mixed one. The recoveries of the pesticides in cabbage samples were observed 92.12%-107.50%. And the recoveries of the mixed pesticides in mineral water samples were observed 86.44%-114.10%. The preliminary study demonstrates that the proposed method has excellent potential application for the safety inspection of food.","PeriodicalId":17253,"journal":{"name":"Journal of the chemical society of pakistan","volume":null,"pages":null},"PeriodicalIF":0.6000,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of the chemical society of pakistan","FirstCategoryId":"92","ListUrlMain":"https://doi.org/10.52568/001189/jcsp/44.06.2022","RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CHEMISTRY, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 1
Abstract
In this paper, a fast detection method for pesticide residues was proposed, and the qualitative and quantitative detection of the pesticide could be got at once by the method of solution of multiple linear regression equations which were obtained by dual wavelength absorbance and fluorescence spectrometry with least squares method. Moreover, it could detect two kinds of mixed pesticides. Four selected pesticides, aldicarb, fenitrothion, fenvalerate, and chlorothalonil were detected by the method. The results shown that there were good linear relationship in the range of 0.01-1 ppm, and R2 > 0.90. And the method could 100% discriminate the four pesticide residues, the limit of detection was below 8 ppb both single one and mixed one. The recoveries of the pesticides in cabbage samples were observed 92.12%-107.50%. And the recoveries of the mixed pesticides in mineral water samples were observed 86.44%-114.10%. The preliminary study demonstrates that the proposed method has excellent potential application for the safety inspection of food.
期刊介绍:
This journal covers different research areas in the field of Chemistry. These include; Analytical Chemistry, Applied Chemistry, Biochemistry, Environmental Chemistry, Industrial Chemistry, Inorganic Chemistry, Organic Chemistry and Physical Chemistry. The journal publishes full length articles and Reviews from researchers in academia in addition to featuring comments. Chemical Research presents short, concise and critical articles offering easy-to-read overviews of basic research and applications in all areas of chemistry.