SINTESIS TiO2/Ti DENGAN TEKNIK ANODISASI DAN UJI AKTIVITAS FOTOKATALIS SEBAGAI ANTIBAKTERI Escherichia coli

Resti Fartiwi, W. Warsidah, A. B. Aritonang
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引用次数: 3

Abstract

Titanium dioxide (TiO2) thin layer on the surface of metal Ti has been successfully synthesized using anodization method by varying the anodization times 30, 45 and 60 minutes. Characterization of TiO2/Ti with FTIR method gives absorption peaks at wave number 457,490 cm-1 and 796,635 cm-1, which is a Ti-O vibration. Visualization TiO2/Ti under SEM showed pores with diameter of 10-45 nm as an indication of the morphology of nanotubes, although the length of tubes have not been obtained. The results of XRD measurement give diffractogram at 2q: 25,337°; 37,891° and 48,074° and characterization DR-UV visible value 3,276 eV band gap which characterize crystalline anatase TiO2 phase. Photocatalytic TiO2/Ti exhibit antibacterial activity Escherichia coli were tested using the method of turbidimetry with a spectrophotometer at wavelength of 600 nm. Photocatalyst TiO2/Ti which are synthesized by anodizing process for 60 minutes have inhibitory bacterial growth better than synthesized for 30 minutes and 45 minutes.
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以消毒技术和光化活性为抗菌的Escherichia大肠杆菌合成TiO2/Ti
采用阳极氧化法,通过改变阳极氧化时间30min、45min和60min,成功地在金属Ti表面合成了二氧化钛(TiO2)薄层。用FTIR方法表征TiO2/Ti,吸收峰位于波数457,490 cm-1和796,635 cm-1处,为Ti- o振动。TiO2/Ti在SEM下的可视化显示,纳米管的孔径为10-45 nm,虽然没有得到管的长度。XRD测量结果给出了2q: 25,337°处的衍射图;37,891°和48,074°,表征DR-UV可见值为3,276 eV的带隙,表征锐钛矿TiO2相结晶。用分光光度计在600 nm波长处对光催化TiO2/Ti对大肠杆菌的抑菌活性进行了测定。阳极氧化60分钟合成的光催化剂TiO2/Ti抑制细菌生长的效果优于阳极氧化30分钟和45分钟合成的光催化剂TiO2/Ti。
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