Abrupt high grain growth in hydroxyapatite during flash sintering

IF 1.3 4区 材料科学 Q3 MATERIALS SCIENCE, CERAMICS Advances in Applied Ceramics Pub Date : 2022-04-03 DOI:10.1080/17436753.2022.2050665
Jooseong Kim, I. Bajpai, J. Jeon, Kyelim Yun, Jaeick Han, J. Shackelford, Young-Hwan Han, Sukyoung Kim
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Abstract

ABSTRACT The electric flash generated by an electric field aided the sintering of hydroxyapatite (HA) in relatively less time and at lower furnace temperatures than the conventional sintering method. The current work has reported a comparative study to explain thermodynamically the effects of the increasing DC electric field strength at 1000°C and 1100°C sintering furnace temperatures during flash sintering in terms of the grain growth and densification of the HA in air. The abrupt change in current density and conductivity of HA during the flash peak correlates the high grain growth and rapid densification with increasing electric field strength. The increased electric field strength reduced the power dissipation from the HA. The abrupt high-rise grain growth phenomenon during flash sintering might consist of the thermal effect and enhancement in ionic conductivity due to the application of an electric field.
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闪蒸烧结过程中羟基磷灰石晶粒突长
电场产生的电闪有助于羟基磷灰石(HA)在相对较短的时间和较低的炉温下烧结。目前的工作报道了一项比较研究,从热力学角度解释了在1000℃和1100℃烧结炉温度下增加直流电场强度对空气中HA晶粒生长和致密化的影响。在闪峰期间,HA的电流密度和电导率的突变与电场强度的增加有关,这与高晶粒生长和快速致密化有关。电场强度的增加降低了HA的功耗。闪速烧结过程中出现的突高晶粒生长现象可能是由于外加电场的热效应和离子电导率的提高所致。
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来源期刊
Advances in Applied Ceramics
Advances in Applied Ceramics 工程技术-材料科学:硅酸盐
CiteScore
4.40
自引率
4.50%
发文量
17
审稿时长
5.2 months
期刊介绍: Advances in Applied Ceramics: Structural, Functional and Bioceramics provides international coverage of high-quality research on functional ceramics, engineering ceramics and bioceramics.
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