A New Method of Determinated Organochlorine Pesticides in the Surface Water

Li Wu, Chao Tai, T. Zhao, Yuanyuan Wang
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Abstract

In this paper, an apparatus of inert gases-surfactants assistant liquid-liquid extraction(ISALLE) is described. Based on this apparatus, a method for the determination of 20 trace level organochlorine pesticides in the water was developed. The influence of various experiment conditions on the extraction efficiency of ISALLE for the organochlorine pesticides was studied. The linearity in the detecting range is good (R≫0.99) with the detection limits of 0.4-2 ng/L¿and the quantification limits of 4-8 ng/L¿The RSDs were lower than 6.7¿ and the recoveries were 83%-121%. The method had been used to determine the organochlorine pesticides in the surface water with satisfactory results.
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地表水中有机氯农药测定新方法研究
介绍了一种惰性气体-表面活性剂辅助液-液萃取装置(ISALLE)。在此基础上,建立了水中20种痕量有机氯农药的测定方法。研究了不同实验条件对ISALLE萃取有机氯农药效率的影响。在检测范围内线性良好(R < 0.99),检出限为0.4 ~ 2 ng/L,定量限为4 ~ 8 ng/L, rsd < 6.7,加样回收率为83% ~ 121%。该方法已用于地表水中有机氯农药的测定,结果令人满意。
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