MATHEMATICAL AND STATISTICAL MODEL OF CLEANING IN A HIGH-GRADIENT MAGNETIC FIELD OF HYDROGENATED FAT FROM SUSPENDED CATALYST

Vyacheslav N. Tyrtygin, A. A. Deniskovets, A. Labutin
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Abstract

The introduction specifies the object of the study - hydrogenated fat subjected to purification from suspended nickel-containing catalyst in a high-gradient magnetic field. The nickel-containing catalyst, due to the presence of nickel salts in it, is paramagnetic and can be effectively extracted from hydrated fat in the magnetic field by a method of highly gradient magnetic separation. In the experiment technique the magnetic field strength was not less than 600 kA/m, the gradient not less than (20-30)∙104 kA/m2. Based on the results and their discussion, the analysis of empirical dependencies on each factor basis is carried out separately, as well as the construction of classical types of one-dimensional non-linear regression models for each of them.  It is shown that the most statistically reliable are the exponential models. It was found that after purification the content of suspended nickel-containing catalyst in the hydrogenated fat has an inverse proportional dependence on the magnetic field strength, height (length) of the filtration zone and filtration rate. A two-dimensional exponential regression model of the content of the nickel-containing catalyst in the hydrogenated fat in the complex dependence on the rate and height of the filtration zone is built. Based on the experimental data at a certain height of the filtration zone and the selected filtration rate, a mathematical-statistical model of change in the concentration of nickel-containing catalyst depending on the magnetic field strength is made. Using the resulting two-dimensional exponential regression model, it is possible to predict the degree of purification of the salomas from the suspended catalyst depending on the specific tension of the magnetic field and to determine the tension of the magnetic field, at which the concentration of nickel as a result of cleaning will reach an advance value.
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悬浮催化剂氢化脂肪在高梯度磁场下清洗的数学和统计模型
介绍了本研究的对象——在高梯度磁场下从悬浮含镍催化剂中提纯氢化脂肪。含镍催化剂由于镍盐的存在,具有顺磁性,可以采用高梯度磁选的方法在磁场中有效地从水合脂肪中提取。在实验技术中,磁场强度不小于600 kA/m,梯度不小于(20-30)∙104 kA/m2。在此基础上,分别对各因素基础上的经验依赖关系进行了分析,并对各因素分别构建了经典类型的一维非线性回归模型。结果表明,指数模型在统计上最可靠。结果表明,提纯后氢化脂肪中悬浮含镍催化剂的含量与磁场强度、过滤区高度(长度)和过滤速率成反比关系。建立了氢化脂肪中含镍催化剂含量与过滤区速率和过滤区高度关系的二维指数回归模型。根据一定过滤区高度下的实验数据和选定的过滤速率,建立了含镍催化剂浓度随磁场强度变化的数学统计模型。利用所得到的二维指数回归模型,可以根据磁场的比张力来预测悬浮催化剂对灰痣的净化程度,并确定磁场张力,在该张力下,清洗后的镍浓度将达到一个提前值。
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