Experimental approach towards the water contact angle value on the biomaterial alloy Ti6Al4V

M. Hierro-Oliva, A. M. Gallardo-Moreno, A. Rodríguez-Cano, J. Bruque, M. Gónzalez-Martín
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引用次数: 5

Abstract

Abstract In the biomedical field, water contact angle is a useful gauge to follow how a biomaterial surface would interact with the surrounding water-like physiological environment. Ti6Al4V alloy is widely used in orthopedic applications. Nevertheless, the values of its water contact angle reported in the literature show a large dispersion, from 40° up 80°. However, in addition to the expected dependence of the surface wettability on preliminary treatments, the values of the water contact angle on the pristine Ti6Al4V alloy suffers from an important variability and lack of reproducibility. The present research pays attention to this difficulty and proposes a simple experimental procedure to ensure adequate contact angle reproducibility. Controlled passivation growth in mild underwater conditions of freshly polished disks, followed by ultrasonic washing, avoiding the rubbing of the surface, gives average water contact angles of 80° with very low standard deviations also among samples from the same batch.
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Ti6Al4V生物材料合金水接触角数值的实验研究
在生物医学领域,水接触角是跟踪生物材料表面如何与周围水样生理环境相互作用的有用指标。Ti6Al4V合金广泛应用于骨科领域。然而,文献报道的其水接触角值显示出很大的分散,从40°到80°。然而,除了预期的表面润湿性依赖于初步处理之外,原始Ti6Al4V合金的水接触角值存在重要的可变性和缺乏可重复性。本研究注意到这一困难,并提出了一种简单的实验程序,以确保足够的接触角再现性。在温和的水下条件下,对刚抛光过的圆盘进行可控的钝化生长,然后进行超声波洗涤,避免了表面的摩擦,同一批次样品的平均水接触角为80°,标准偏差也很低。
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