Development of a new high-temperature and high-strength polymer gel for plugging fractured reservoirs

IF 2.6 Q3 ENERGY & FUELS Upstream Oil and Gas Technology Pub Date : 2020-10-01 DOI:10.1016/j.upstre.2020.100014
Zhi-yong Li , Xin-gang Li , Kun Du , Hua-kang Liu
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引用次数: 15

Abstract

In fractured reservoirs, the fracture size distribution is wide with strong heterogeneity, and wide fractures are not easily plugged. Conventional plugging methods have limitations in reservoir leakage problems. The matching degree of plugging materials and reservoir fractures is relatively low once small particles are transported deep into the reservoir, which can finally cause reservoir damage. Gel plays an important role in the temporary plugging of fractured reservoirs. However, there are currently few mature gel systems that can maintain good rheological properties at room temperature, good gelation at a high temperature and a sustained plugging strength. In this paper, a high-temperature and high-strength (HTHS) gel system was developed, and its properties were evaluated in the laboratory. The gel is cross-linked by covalent bonds, and its temperature resistance can reach 150 °C. Rheological and gelation tests show that the gel solution exhibits good rheological properties at room temperature and can cross-link into a gel at high temperatures. The gelation time could be flexibly adjusted from 4 to 10 h. The gel has good expansibility and can entirely fill fractures. The plugging test reveals that the plugging pressure can reach 0.25 MPa/cm in a 5-mm fracture, and the strength stability can be maintained for one month. Gelation stability can be maintained in the presence of formation water and drilling fluid. The gel has a good self-breaking capability after a period of time and does not affect reservoir production. This study can provide a plugging solution for fractured reservoirs at high temperatures and pressures.

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裂缝性储层封堵用高温高强聚合物凝胶的研制
裂缝性储层裂缝尺寸分布宽,非均质性强,宽裂缝不易堵塞。常规封堵方法在油藏泄漏问题中存在局限性。一旦小颗粒运移到储层深处,堵料与储层裂缝的匹配度较低,最终造成储层破坏。凝胶在裂缝性储层的临时封堵中起着重要作用。然而,目前很少有成熟的凝胶体系能够在室温下保持良好的流变性能,在高温下保持良好的凝胶性,并保持持续的封堵强度。本文研制了一种高温高强(HTHS)凝胶体系,并对其性能进行了实验室评价。凝胶通过共价键交联,耐温可达150℃。流变学和凝胶实验表明,该凝胶溶液在室温下具有良好的流变特性,在高温下可交联成凝胶。凝胶时间可在4 ~ 10 h之间灵活调节,凝胶具有良好的膨胀性,可完全填充裂缝。封堵试验结果表明,在5mm裂缝中,封堵压力可达0.25 MPa/cm,强度稳定可保持1个月。在地层水和钻井液存在的情况下,仍能保持凝胶稳定性。该凝胶在一段时间后具有良好的自破能力,不影响储层的生产。该研究为高温高压条件下裂缝性油藏的封堵提供了一种解决方案。
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