POWGEN: a third-generation high resolution high-throughput powder diffraction instrument at the Spallation Neutron Source

A. Huq, J. P. Hodges, L. Heroux, O. Gourdon
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引用次数: 43

Abstract

Powgen represents a departure from previous designs for a time-of-flight powder diffractometer at a spallation neutron source and may be considered a third-generation design. The instrument is optimized for both parametric studies of materials under a wide range of conditions (T, P, H, flowing gases, etc) and ab-initio crystal structure determinations of complex solid-state materials with asymmetric unit-cells of the order {approx}1500 {angstrom}{sup 3}. The geometric design of the instrument allows for all detected scattered neutrons to be focused onto a single diffraction profile yielding high count rate while preserving good resolution {Delta}d/d = 0.0015 at a d = 1 {angstrom}.
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POWGEN:第三代高分辨率高通量散裂中子源粉末衍射仪
Powgen代表了与先前设计的散裂中子源飞行时间粉末衍射仪的不同,可以被认为是第三代设计。该仪器经过优化,可用于各种条件下(T、P、H、流动气体等)材料的参数研究,以及具有{约}1500{埃}{sup 3}阶的不对称单元胞的复杂固态材料的从头算晶体结构测定。仪器的几何设计允许将所有检测到的散射中子集中在单一衍射剖面上,产生高计数率,同时在d = 1{埃}处保持良好的分辨率{Delta}d/d = 0.0015。
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来源期刊
CiteScore
1.47
自引率
0.00%
发文量
0
审稿时长
3 months
期刊介绍: Zeitschrift für Kristallographie International journal for structural, physical, and chemical aspects of crystalline materials ISSN 0044-2968 Founded in 1877 by Paul Groth Zeitschrift für Kristallographie is one of the world’s oldest scientific journals. In original papers, letters and review articles it presents results of theoretical or experimental study on crystallography.
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