One pot synthesis of MoO3/MoS2 composite and investigation on its electrochemical charge storage properties

Nikhitha Joseph, A. C. Bose
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引用次数: 4

Abstract

Transition metal compounds are widely used in electrochemical energy storage application due to their variable oxidation state. Molybdenum disulfide is one of the important transition metal dichalcogenide, with layered structure similar to graphene. Here we report one-pot synthesis of MoS2/MoO3 nanocomposite for the electrochemical energy storage electrode application. Crystal structure of the as-prepared composite is confirmed by XRD analysis. The achieved maximum specific capacitance for MoS2/MoO3 nanocomposite is 303 F/g at 1 A/g current density. An excellent rate capability of 77.2% is attained at 10 A/g. The enhanced specific capacitance and good capacitive retention is due to the collective contribution from both the material. Hence we propose MoS2/MoO3 nanocomposite as an efficient material for electrochemical energy storage application.Transition metal compounds are widely used in electrochemical energy storage application due to their variable oxidation state. Molybdenum disulfide is one of the important transition metal dichalcogenide, with layered structure similar to graphene. Here we report one-pot synthesis of MoS2/MoO3 nanocomposite for the electrochemical energy storage electrode application. Crystal structure of the as-prepared composite is confirmed by XRD analysis. The achieved maximum specific capacitance for MoS2/MoO3 nanocomposite is 303 F/g at 1 A/g current density. An excellent rate capability of 77.2% is attained at 10 A/g. The enhanced specific capacitance and good capacitive retention is due to the collective contribution from both the material. Hence we propose MoS2/MoO3 nanocomposite as an efficient material for electrochemical energy storage application.
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一锅法合成MoO3/MoS2复合材料及其电化学电荷存储性能研究
过渡金属化合物因其易氧化态而在电化学储能领域得到了广泛的应用。二硫化钼是重要的过渡金属二硫化物之一,具有类似石墨烯的层状结构。本文报道了一锅法合成用于电化学储能电极的MoS2/MoO3纳米复合材料。通过XRD分析证实了复合材料的晶体结构。在电流密度为1 A/g时,MoS2/MoO3纳米复合材料的最大比电容为303 F/g。在10 A/g时,达到77.2%的出色速率能力。增强的比电容和良好的电容保持是由于这两种材料的共同贡献。因此,我们提出了MoS2/MoO3纳米复合材料作为一种高效的电化学储能材料。过渡金属化合物因其易氧化态而在电化学储能领域得到了广泛的应用。二硫化钼是重要的过渡金属二硫化物之一,具有类似石墨烯的层状结构。本文报道了一锅法合成用于电化学储能电极的MoS2/MoO3纳米复合材料。通过XRD分析证实了复合材料的晶体结构。在电流密度为1 A/g时,MoS2/MoO3纳米复合材料的最大比电容为303 F/g。在10 A/g时,达到77.2%的出色速率能力。增强的比电容和良好的电容保持是由于这两种材料的共同贡献。因此,我们提出了MoS2/MoO3纳米复合材料作为一种高效的电化学储能材料。
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