S. Voitekhovich, M. M. Degtyarik, A. Lyakhov, L. Ivashkevich, Yuri V. Grigoriev, O. Ivashkevich
{"title":"Synthesis and structure of novel tripodal ligands based on tetrazol-5-thioles","authors":"S. Voitekhovich, M. M. Degtyarik, A. Lyakhov, L. Ivashkevich, Yuri V. Grigoriev, O. Ivashkevich","doi":"10.33581/2520-257x-2022-2-10-18","DOIUrl":null,"url":null,"abstract":"Novel tripodal ligands (R1N4CS)3CH, where R1 = Me, Ph, were synthesised by alkylation of 1-R-tetrazol-5-thioles with iodoform in alkaline media. These ligands were identified based on data of elemental analysis, nuclear magnetic resonance spectroscopy, thermal analysis, and X-ray diffraction analysis of single crystals.","PeriodicalId":17303,"journal":{"name":"Journal of the Belarusian State University. Chemistry","volume":"19 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2022-08-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of the Belarusian State University. Chemistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.33581/2520-257x-2022-2-10-18","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
Abstract
Novel tripodal ligands (R1N4CS)3CH, where R1 = Me, Ph, were synthesised by alkylation of 1-R-tetrazol-5-thioles with iodoform in alkaline media. These ligands were identified based on data of elemental analysis, nuclear magnetic resonance spectroscopy, thermal analysis, and X-ray diffraction analysis of single crystals.
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