Sılıcon Based Gel to Shut-Off of Water in the Well-Bore

Maharat Huseynov, S. Tapdiqov, Fariz Ahmad, Sevda Kazimova
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Abstract

The quality of gel - based silicon, which forms an insulating content to prevent water and sand in oil and gas wells, have been improved. Based on the reaction between the liquid glass and hydrochloric acid, the optimal concentration of the initial reagents for the formation of the gel process was determined. The rheology, initial and final setting time of the silicon based gel, and the temperature dependencies of the gel forming process were also studied by adding 0.1-1.0% (mass ratio) of urea as cross-linking to the Na2SiO3/HCl solution. At the same time, the impact of the obtained gel of the permeability of the rock pores was determined and the filtration characteristics were studied. It has been determined that with 0.1-0.8% mass concentration of the urea added to the Na2SiO3/HCl solution, the setting time of the gel could be regulated according to the well-layer regime. The resulting silicone-based gel can be used as an injection solution that can set in 3-22 hours in oil and gas wells between the temperature of 20-80 °C.
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Sılıcon基凝胶封堵井筒水
胶基硅在油气井中形成绝缘成分,起到防水防砂的作用,其质量得到了改善。根据液体玻璃与盐酸的反应,确定了凝胶形成过程中初始试剂的最佳浓度。通过在Na2SiO3/HCl溶液中加入0.1 ~ 1.0%(质量比)的尿素作为交联剂,研究了硅基凝胶的流变性、初凝和终凝时间以及凝胶形成过程的温度依赖性。同时,测定所得凝胶对岩石孔隙渗透率的影响,研究其过滤特性。结果表明,在Na2SiO3/HCl溶液中加入0.1-0.8%质量浓度的尿素,凝胶的凝固时间可根据井层结构进行调节。所得的硅基凝胶可以作为注入溶液,在温度为20-80°C的油气井中可以在3-22小时内坐封。
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