Study on synthesizing green reaction media for biodiesel production

Jianjun Yang, W. Guan, Hongrong Che
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Abstract

We mainly investigated the synthesis process of ionic liquids, and the parameters were optimized. By means of FT-IR and NMR spectroscopy analysis, we determined that the product synthesized was the purpose product [BMIM] [BF4]. By means of the thermal analysis for its thermal stability, we found that [BMIM][BF4] was suit to be a new reaction media for biodiesel production. Lipase catalyzed synthesis of biodiesel in [BMIM][BF4] reaction media. After 10 batches of reaction, 67.7% FAMEs yield in [BMIM][BF4] reaction media was superior to 5.5% FAMEs yield in tert-butyl alcohol reaction media.
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生物柴油绿色反应介质的合成研究
主要研究了离子液体的合成工艺,并对工艺参数进行了优化。通过FT-IR和NMR分析,我们确定合成的产物为目的产物[BMIM] [BF4]。通过对其热稳定性的热分析,发现[BMIM][BF4]适合作为生产生物柴油的新型反应介质。脂肪酶催化[BMIM][BF4]反应介质合成生物柴油。经过10批反应,在[BMIM][BF4]反应介质中,FAMEs的收率为67.7%,优于在叔丁醇反应介质中,FAMEs的收率为5.5%。
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