Saraca indica as reducing agent for synthesis of modified copper oxide nanoparticles at low temperatures using green synthesis method

S. Samhitha, B. A. Kumar, G. Raghavendra, P. Bindu
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引用次数: 2

Abstract

Copper Oxide (CuO) being one of the transition metal oxide has an unfathomable number of applications such as photoconductive functionalities, industrial and medical applications. The current study aims at the synthesis of CuO nanoparticles with the use of Saraca Indica (Ashoka) leaf extract, which acts as a reducing agent. The experimental conditions were optimized for nano-range synthesis of CuO particles. The obtained CuO nanoparticles have been characterized using various analytical techniques such as SEM, FTIR, XRD. Scanning Electron Microscope images revealed that the nanoparticles are in petal like shaped structures, having an average crystallite size of~ 14 nm. The XRD graph confirmed that the obtained CuO nanoparticles have monoclinic structure and has a preferred Morphology Index. The FTIR plot further confirmed the presence of Cu-O bonding with a slight modifications with functional groups. CuO nanoparticles of different properties and dimensions can be prepared with the help of different leaf concentrations and Copper salts. This work provides a simple, environmental friendly, tailor made and a cost effective way of synthesizing CuO nanoparticles using Green method.
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采用绿色合成法在低温下合成改性氧化铜纳米颗粒
氧化铜(CuO)作为过渡金属氧化物之一,在光导功能、工业和医疗等方面有着不可估量的应用。目前的研究旨在利用印度树(Ashoka)叶提取物作为还原剂合成CuO纳米颗粒。优化了纳米范围合成氧化铜颗粒的实验条件。利用扫描电镜(SEM)、红外光谱(FTIR)、x射线衍射(XRD)等分析技术对制备的纳米CuO进行了表征。扫描电镜图像显示,纳米颗粒呈花瓣状结构,平均晶粒尺寸为~ 14 nm。XRD图证实了制备的CuO纳米颗粒具有单斜晶型结构,具有较好的形貌指数。FTIR图进一步证实了Cu-O键的存在,并与官能团进行了轻微的修饰。不同的叶片浓度和铜盐可以制备出不同性质和尺寸的CuO纳米颗粒。这项工作提供了一种简单、环保、定制和成本有效的方法来合成CuO纳米颗粒。
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