D. Le, A. Bougrine, O. Duclos, V. Pasquet, H. Delalu
{"title":"A New Strategy for the Synthesis of Monomethylhydrazine Using the Raschig Process","authors":"D. Le, A. Bougrine, O. Duclos, V. Pasquet, H. Delalu","doi":"10.4236/aces.2021.113014","DOIUrl":null,"url":null,"abstract":"A new strategy for the development of monomethylhydrazine (MMH) using the \nRaschig process is discussed in this publication. The determination of optimal \nconditions for the synthesis of MMH required the development of a kinetic \nmodel. In order to validate the results of the calculation, a device for \nsynthesis under pressure (13 bar) by direct injection of the stoichiometric \nmonochloramine, synthesized using microreactor technology, into monomethylamine \n(MMA) was developed. The experimental data, in accordance with the theoretical \nresults of the kinetic model, make it possible to establish a new process for \nthe synthesis of monomethylhydrazine.","PeriodicalId":7332,"journal":{"name":"Advances in Chemical Engineering and Science","volume":"1 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2021-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Advances in Chemical Engineering and Science","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.4236/aces.2021.113014","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
Abstract
A new strategy for the development of monomethylhydrazine (MMH) using the
Raschig process is discussed in this publication. The determination of optimal
conditions for the synthesis of MMH required the development of a kinetic
model. In order to validate the results of the calculation, a device for
synthesis under pressure (13 bar) by direct injection of the stoichiometric
monochloramine, synthesized using microreactor technology, into monomethylamine
(MMA) was developed. The experimental data, in accordance with the theoretical
results of the kinetic model, make it possible to establish a new process for
the synthesis of monomethylhydrazine.