Direct observation of the processes near particle-to-particle contacts at electric pulse consolidation of titanium powder

A. Rogachev, S. Vadchenko, V. Kudryashov, A. Shchukin, M. Alymov
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Abstract

Direct high-speed micro-video records prove the existence of highly overheated zones at the contacts of powder particles during short (~ 1 ms) electric current pulses. The value of overheating can exceed 1600 degrees and lead to the formation of liquid-phase sintering necks, the dimensions of which are well correlated with the size of the overheated zones. The micro-uniformity of the temperature field in the electric pulse heating allow understanding the unusually high consolidation rates of powder materials observed in spark plasma sintering.
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直接观察钛粉电脉冲固结时颗粒间接触过程
直接高速微视频记录证明,在短电流(~ 1ms)脉冲作用下,粉末颗粒接触处存在高度过热区。过热值可超过1600度,导致液相烧结颈的形成,其尺寸与过热区的大小有很好的相关性。电脉冲加热温度场的微观均匀性使我们能够理解火花等离子烧结中观察到的粉末材料异常高的固结率。
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