Mini Electrode Based on Chitosan-Activated Carbon Membrane for Detection of Paracetamol in Herbal Medicine

Ani Mulyasuryani, Rachmat Triandi, Zainul Abidin
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Abstract

A tube type mini electrode has been made to detect paracetamol levels in herbal medicine, the electrode is made of a glass tube with a diameter of 0.7 cm, a length of 3 cm. As the membrane is a mixture of chitosan, activated carbon from rice husk, and cetyl trimethyl ammonium (CTA)-paracetamol. The internal solution is a standard solution of 0.01 M paracetamol in a solution of phosphoric acid pH 2. The average sensitivity of the paracetamol sensor is (22.60 ± 0.01) mV/decade in a linear concentration range of 10-6 – 5x10-3 M, with an average recovery of (90.6 ± 0.5) %. Paracetamol sensor electrodes can be applied to samples of herbal medicine on the market, with an average error of (9.4 ± 0.1) %.
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壳聚糖-活性炭膜微型电极检测中草药中扑热息痛
研制了一种用于检测草药中扑热息痛含量的管状微型电极,该电极由直径为0.7厘米、长度为3厘米的玻璃管制成。由于膜是壳聚糖、稻壳活性炭和十六烷基三甲基铵(CTA)-扑热息痛的混合物。内溶液为0.01 M扑热息痛在pH为2的磷酸溶液中的标准溶液。对乙酰氨基酚传感器在10-6 ~ 5 × 10-3 M线性浓度范围内的平均灵敏度为(22.60±0.01)mV/ 10年,平均回收率为(90.6±0.5)%。对乙酰氨基酚传感器电极可应用于市场上的草药样品,平均误差为(9.4±0.1)%。
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