Structure and phase constitution of graphite-loaded reaction-bonded sic

O. Sorokin, I. O. Belyachenkov, A. S. Chainikova, S. V. Zhitnyuk, P. Medvedev
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Abstract

The influence of porous SiC preforms densities for the siliconizing process on the structure and phase constitution of graphite-loaded reaction-bonded SiC (G-SiSiC) was studied. It was found that varying the densities of porous SiC preforms containing artificial graphite of similar grain size with the dimensions less than 25 mm (in height or diameter) can lead to the G-SiSiC samples with low free Si content (less 4 wt.%.). It was also shown that reaction sintering of G-SiSiC samples with the optimized densities during the siliconizing process results in the formation of a dense fine-grained SiC layer. Moreover, during the siliconizing process, a dense SiC gradient matrix is formed in which graphite and Si inclusions are uniformly dispersed in bulk.
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石墨负载反应键合碳化硅的结构与相组成
研究了硅化过程中多孔碳化硅预制体密度对石墨负载反应键合碳化硅(G-SiSiC)结构和相组成的影响。结果表明,在相似晶粒尺寸且尺寸小于25 mm(高度或直径)的人造石墨的多孔SiC预制体中,改变密度可以得到游离Si含量较低(小于4 wt.%)的G-SiSiC样品。结果表明,在硅化过程中,以优化密度对G-SiSiC样品进行反应烧结,可形成致密的细晶SiC层。在硅化过程中,石墨和硅夹杂体均匀分散,形成致密的SiC梯度基体。
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