X-ray fluorescence spectrometry: An alternative technique for analysis of waste

M. Scapin, M. C. Tessari-Zampieri, S. Guilhen, M. Cotrim
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Abstract

This study aims to develop reliable analytical methodology that is, cost-effective, and requires minimal sample quantity to quantify uranium content in nuclear waste and others. The Energy Dispersive X-ray Fluorescence Spectrometry (EDXRF) technique was used, and a rigorous comparison was made between the fundamental parameters (FP) method and the empirical (EMP) method. Statistical evaluation of results demonstrated that the FP method showed a satisfactory level of confidence for precision and limit of quantification.
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x射线荧光光谱法:废物分析的一种替代技术
这项研究的目的是发展可靠的分析方法,即具有成本效益,并且需要最少的样本量来量化核废料和其他废料中的铀含量。采用能量色散x射线荧光光谱(EDXRF)技术,对基本参数法(FP)和经验法(EMP)进行了严格比较。统计评价结果表明,FP方法在精密度和定量限方面具有令人满意的置信水平。
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