Fabrication of Vinyl Functionalised Multiwalled Carbon Nanotubes for the Removal of Organic Pollutant

T.R. Sreelakshmi, T. Sajini, B. Mathew
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Abstract

A novel and convenient approach for the fabrication of vinyl functionalized multiwalled carbon nanotube (MWCNT) as a sorbent for organic pollutant is described in this article. In this method, the purified MWCNT is functionalized via a non-covalent strategy using 9-vinyl anthracene, fluorescent active species. The synthesised nanotube was characterised using various techniques such as Fourier transform infrared spectroscopy (FT-IR), UV-Vis. spectroscopic analysis, scanning electron microscopy (SEM), X-ray diffraction technique (XRD), thermogravimetric analysis (TGA), transmission electron microscopy (TEM) and Raman spectroscopy. Effects of concentration, pH and time for the functionalization of MWCNTs were investigated through photoluminescence (PL) studies. The resulting vinyl functionalized MWCNT will act as a promising adsorbent for organic pollutants like p-chlorobenzoic acid.
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乙烯基功能化多壁碳纳米管去除有机污染物的制备
本文介绍了一种制备乙烯基功能化多壁碳纳米管(MWCNT)作为有机污染物吸附剂的新方法。在这种方法中,纯化的MWCNT通过非共价策略使用9-乙烯基蒽,荧光活性物质功能化。利用傅里叶变换红外光谱(FT-IR)、UV-Vis等多种技术对合成的纳米管进行了表征。光谱分析、扫描电子显微镜(SEM)、x射线衍射技术(XRD)、热重分析(TGA)、透射电子显微镜(TEM)和拉曼光谱。通过光致发光(PL)研究了浓度、pH和时间对MWCNTs功能化的影响。由此产生的乙烯基功能化MWCNT将作为对氯苯甲酸等有机污染物的吸附剂。
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