Toward Deep Diversion for Waterflooding and EOR: From Representative Delayed Gelation to Practical Field-Trial Design

A. AlSofi, W. Dokhon
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Abstract

Conformance control via near-wellbore mechanical and chemical treatments is well established. However, for extreme heterogeneities, effective conformance control mandates deep treatments. Such deep treatments or diversion would sustain sweep enhancement far from wells, deep into the reservoir. Deep diversion is even more mandatory for enhanced oil recovery (EOR) to assure the expensive injectants optimally contact the remaining oil. In this paper, we comprehensively present efforts to research, develop, and trial a crosslinked-gel system for deep diversion. We started by reviewing conformance control options including crosslinked systems. The review supported the immaturity of deep conformance control. Various gel-based solutions, especially preformed particle gels (PPGs) and colloidal dispersed gels (CDGs), were proposed; however, diversion effects were not clearly illustrated. For crosslinked-gels, all systems exhibited fast gelation, something suitable for near-wellbore treatments. We then studied the key crosslinked systems. We characterized their behavior using rheometry, bottle tests, and single-phase corefloods. We assessed their potential through oil-displacement corefloods in artificially fractured cores with and without in-situ imaging. In-house studies, on key gel systems demonstrated the feasibility of gels to affect diversion and enhance recovery but corroborated the extreme challenge to design systems with delayed gelation. To assure representative gelation, we developed, and utilized a continuous bi-directional injection protocol to assess gelation times in-situ. From there, we collaboratively developed, and characterized a unique delayed-gelation formulation. The collaborative study addressed this challenge where systems with delayed gelation were developed. In-situ gelation time estimation confirmed this delayed gelation capacity. Further corefloods addressed the key uncertainties including injectivity losses, limited propagation, and ineffective blockage. Simulations were performed to assess the process feasibility.The simulation studies supported the utility of deep diversion treatments. Simulation also guided the initial design of a trial. We focused on the design of a practical field trial.For further derisking, the first trial was optimized to serve as a practical proof-of-concept. Taking into account economics, success measurement, flow assurance, and depth of placement, we diverged from a trial where we observe deep diversion (and infer delayed gelation and effective blockage) then converged into a trial where we infer deep diversion (by observing delayed gelation and effective blockage). With that, we screened candidates with a clear hierarchy of screening criteria. Through this program, and for the first-time in the industry, we demonstrate the potential utility and feasibility of a crosslinked-gel system for deep diversion applications. This potential is supported by comprehensive experimentation including novel in-situ estimation of gelation times. Finally, a consistent workflow to design a practical field trial is laid out. This, in terms of design considerations and hierarchal screening, is believed to be of extreme value to the practicing reservoir engineers.
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向水驱和提高采收率的深层导流:从典型的延迟胶凝到实际的现场试验设计
通过近井机械和化学处理控制井眼一致性已经建立。然而,对于极端的异质性,有效的一致性控制要求进行深度处理。这种深层处理或转移可以维持远离井、深入储层的波及效果。为了提高采收率(EOR),为了确保昂贵的注入剂与剩余油最佳地接触,深层分流就更加必要了。本文全面介绍了一种用于深层导流的交联凝胶体系的研究、开发和试验。我们首先回顾了包括交联系统在内的一致性控制选项。审查支持深度一致性控制的不成熟。提出了各种凝胶基溶液,特别是预成型颗粒凝胶(PPGs)和胶体分散凝胶(CDGs);然而,转移效应并没有得到清楚的说明。对于交联凝胶,所有体系都表现出快速凝胶化,适用于近井处理。然后我们研究了关键的交联体系。我们使用流变学、瓶子测试和单相岩心驱油来表征它们的行为。我们通过人工压裂岩心的驱油驱心来评估它们的潜力,有和没有进行原位成像。对关键凝胶体系的内部研究证明了凝胶影响转向和提高采收率的可行性,但也证实了设计延迟凝胶体系的极端挑战。为了确保具有代表性的凝胶,我们开发并使用了连续双向注射方案来评估原位凝胶时间。从那里,我们合作开发了一种独特的延迟凝胶配方。合作研究解决了这一挑战,开发了延迟凝胶化系统。原位凝胶时间估计证实了这种延迟凝胶能力。进一步的岩心驱油解决了关键的不确定性,包括注入损失、有限扩散和无效堵塞。通过仿真来评估该工艺的可行性。模拟研究支持深度导流处理的实用性。仿真还指导了试验的初步设计。我们专注于设计一个实际的现场试验。为了进一步降低风险,第一次试验被优化为实际的概念验证。考虑到经济、成功测量、流量保证和放置深度,我们从观察深层分流(并推断延迟凝胶化和有效堵塞)的试验中分离出来,然后融合到推断深层分流(通过观察延迟凝胶化和有效堵塞)的试验中。有了这些,我们就用清晰的等级筛选标准筛选候选人。通过这个项目,我们首次在业内证明了交联凝胶体系在深度导流应用中的潜在效用和可行性。这种潜力得到了综合实验的支持,包括新的凝胶时间的原位估计。最后,给出了设计实际现场试验的统一工作流程。就设计考虑和分层筛选而言,这被认为对实践油藏工程师具有极大的价值。
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