Some New Heterocyclisations Based on N-(2,2-dichloro-1-isothiocyanatoethyl)benzamide Derivatives

IF 0.4 Q4 CHEMISTRY, MULTIDISCIPLINARY Acta Chemica Iasi Pub Date : 2019-06-01 DOI:10.2478/achi-2019-0005
Ihor O. Pokotylo, P. Zadorozhnii, V. Kiselev, O. V. Okhtina, A. V. Kharchenko
{"title":"Some New Heterocyclisations Based on N-(2,2-dichloro-1-isothiocyanatoethyl)benzamide Derivatives","authors":"Ihor O. Pokotylo, P. Zadorozhnii, V. Kiselev, O. V. Okhtina, A. V. Kharchenko","doi":"10.2478/achi-2019-0005","DOIUrl":null,"url":null,"abstract":"Abstract Based on the readily available N-(2,2-dichloro-1-(2-(4-methylbenzoyl)-hydrazine-1-carbothioamido)ethyl)benzamide, the corresponding N-(2,2-dichloro-1-((5-(p-tolyl)-1,3,4-oxadiazol-2-yl)amino)ethyl)benzamide and 5-(p-tolyl)-1,3,4-thiadiazol-2-amine were obtained. The products were received in acceptable yields and were isolated from the reaction mixture without any particular difficulty. The structure of the compounds obtained was confirmed by 1H, 13C NMR spectroscopy and mass spectrometry data.","PeriodicalId":6958,"journal":{"name":"Acta Chemica Iasi","volume":"23 1","pages":"65 - 72"},"PeriodicalIF":0.4000,"publicationDate":"2019-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Acta Chemica Iasi","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.2478/achi-2019-0005","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CHEMISTRY, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 0

Abstract

Abstract Based on the readily available N-(2,2-dichloro-1-(2-(4-methylbenzoyl)-hydrazine-1-carbothioamido)ethyl)benzamide, the corresponding N-(2,2-dichloro-1-((5-(p-tolyl)-1,3,4-oxadiazol-2-yl)amino)ethyl)benzamide and 5-(p-tolyl)-1,3,4-thiadiazol-2-amine were obtained. The products were received in acceptable yields and were isolated from the reaction mixture without any particular difficulty. The structure of the compounds obtained was confirmed by 1H, 13C NMR spectroscopy and mass spectrometry data.
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
基于N-(2,2-二氯-1-异硫氰酸乙酯)苯酰胺衍生物的一些新的杂环化合物
摘要以现有的N-(2,2-二氯-1-(2-(4-甲基苯甲酰)-肼-1-碳硫氨基)乙基)苯酰胺为基础,合成了相应的N-(2,2-二氯-1-(5-(对苯基)-1,3,4-恶二唑-2-基)氨基)乙基)苯酰胺和5-(对苯基)-1,3,4-噻二唑-2-胺。产品以可接受的收率接收,并从反应混合物中分离出来,没有任何特别的困难。所得化合物的结构经1H、13C NMR和质谱数据证实。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
求助全文
约1分钟内获得全文 去求助
来源期刊
Acta Chemica Iasi
Acta Chemica Iasi CHEMISTRY, MULTIDISCIPLINARY-
自引率
0.00%
发文量
0
审稿时长
12 weeks
期刊最新文献
ANTIPLASMODIAL ACTIVITY AND PHYTOCHEMICAL ANALYSIS OF EXTRACTS FROM THE ROOTS AND STEM BARK OF JATROPHA CURCAS TYPE 2 DIABETES MULLITUS PATIENTS WITH AND WITHOUT HYPERTENSION: XANTHINE OXIDASE ACTIVITY AND URIC ACID CONCENTRATION SPECTROPHOTOMETRIC COLORIMETRIC DETERMINATION FOR RESORCINOL DURING SILVER NANOPARTICLES FORMATION WITH A FOCUSED PLASMON RESONANCE SURFACE USING POLYVINYL PYRROLIDONE AS STABILIZER UV–VISIBLE SPECTROPHOTOMETRIC DETERMINATION OF CHLORPROMAZINE HYDROCHLORIDE FROM PHARMACEUTICALS USING PLATINUM (IV) CHLORIDE STUDY ROLE OF INTERLEUKIN-10 AND INTERLEUKIN-1Α ON PATIENTS WITH PROSTATITIS IN BABYLON PROVINCE, IRAQ
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1