Nickel oxide (NiO)/reduced graphene oxide (RGO) composite modified carbon paste electrode as an electrochemical sensor for the sensitive determination of dopamine

T. Joseph, V. K. Sona, A. Aiswarya, Faseeha Abdul Rasheed, Nygil Thomas
{"title":"Nickel oxide (NiO)/reduced graphene oxide (RGO) composite modified carbon paste electrode as an electrochemical sensor for the sensitive determination of dopamine","authors":"T. Joseph, V. K. Sona, A. Aiswarya, Faseeha Abdul Rasheed, Nygil Thomas","doi":"10.1063/1.5130358","DOIUrl":null,"url":null,"abstract":"A simple, nickel oxide/reduced graphene oxide composite modified carbon paste electrode (NiO/RGO-MCPE) was fabricated as an electrochemical sensor for the sensitive determination of Dopamine (DA). Hummers method and coprecipitation followed by reduction method were used for facile, simple and cost-effective preparation for the modifier graphite oxide and NiO/RGO composite respectively. The composite was characterized by using PXRD, FT-IR and TG-DSC. The greater surface area of NiO/RGO composite improves the performance towards DA. The NiO/RGO-MCPE possesses better electrochemical activity in Cyclic Voltammetry (CV) and Differential Pulse Voltammetry (DPV). The developed sensor shows good reproducibility, and stability. Detection limit of DA was determined from differential pulse voltammetry (DPV) and found to be 8.3 nM.A simple, nickel oxide/reduced graphene oxide composite modified carbon paste electrode (NiO/RGO-MCPE) was fabricated as an electrochemical sensor for the sensitive determination of Dopamine (DA). Hummers method and coprecipitation followed by reduction method were used for facile, simple and cost-effective preparation for the modifier graphite oxide and NiO/RGO composite respectively. The composite was characterized by using PXRD, FT-IR and TG-DSC. The greater surface area of NiO/RGO composite improves the performance towards DA. The NiO/RGO-MCPE possesses better electrochemical activity in Cyclic Voltammetry (CV) and Differential Pulse Voltammetry (DPV). The developed sensor shows good reproducibility, and stability. Detection limit of DA was determined from differential pulse voltammetry (DPV) and found to be 8.3 nM.","PeriodicalId":20725,"journal":{"name":"PROCEEDINGS OF THE INTERNATIONAL CONFERENCE ON ADVANCED MATERIALS: ICAM 2019","volume":"201 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2019-10-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"PROCEEDINGS OF THE INTERNATIONAL CONFERENCE ON ADVANCED MATERIALS: ICAM 2019","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1063/1.5130358","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 3

Abstract

A simple, nickel oxide/reduced graphene oxide composite modified carbon paste electrode (NiO/RGO-MCPE) was fabricated as an electrochemical sensor for the sensitive determination of Dopamine (DA). Hummers method and coprecipitation followed by reduction method were used for facile, simple and cost-effective preparation for the modifier graphite oxide and NiO/RGO composite respectively. The composite was characterized by using PXRD, FT-IR and TG-DSC. The greater surface area of NiO/RGO composite improves the performance towards DA. The NiO/RGO-MCPE possesses better electrochemical activity in Cyclic Voltammetry (CV) and Differential Pulse Voltammetry (DPV). The developed sensor shows good reproducibility, and stability. Detection limit of DA was determined from differential pulse voltammetry (DPV) and found to be 8.3 nM.A simple, nickel oxide/reduced graphene oxide composite modified carbon paste electrode (NiO/RGO-MCPE) was fabricated as an electrochemical sensor for the sensitive determination of Dopamine (DA). Hummers method and coprecipitation followed by reduction method were used for facile, simple and cost-effective preparation for the modifier graphite oxide and NiO/RGO composite respectively. The composite was characterized by using PXRD, FT-IR and TG-DSC. The greater surface area of NiO/RGO composite improves the performance towards DA. The NiO/RGO-MCPE possesses better electrochemical activity in Cyclic Voltammetry (CV) and Differential Pulse Voltammetry (DPV). The developed sensor shows good reproducibility, and stability. Detection limit of DA was determined from differential pulse voltammetry (DPV) and found to be 8.3 nM.
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
氧化镍(NiO)/还原氧化石墨烯(RGO)复合修饰碳糊电极作为电化学传感器灵敏测定多巴胺
制备了一种简单的氧化镍/还原氧化石墨烯复合修饰碳糊电极(NiO/RGO-MCPE)作为电化学传感器,用于多巴胺(DA)的灵敏测定。采用Hummers法和共沉淀法分别制备了改性剂氧化石墨和NiO/RGO复合材料,制备方法简便、成本低。采用PXRD、FT-IR和TG-DSC对复合材料进行了表征。NiO/RGO复合材料的表面积越大,其抗DA性能越好。NiO/RGO-MCPE在循环伏安法(CV)和差分脉冲伏安法(DPV)中具有较好的电化学活性。所研制的传感器具有良好的重现性和稳定性。采用差分脉冲伏安法(DPV)测定DA的检出限为8.3 nM。制备了一种简单的氧化镍/还原氧化石墨烯复合修饰碳糊电极(NiO/RGO-MCPE)作为电化学传感器,用于多巴胺(DA)的灵敏测定。采用Hummers法和共沉淀法分别制备了改性剂氧化石墨和NiO/RGO复合材料,制备方法简便、成本低。采用PXRD、FT-IR和TG-DSC对复合材料进行了表征。NiO/RGO复合材料的表面积越大,其抗DA性能越好。NiO/RGO-MCPE在循环伏安法(CV)和差分脉冲伏安法(DPV)中具有较好的电化学活性。所研制的传感器具有良好的重现性和稳定性。采用差分脉冲伏安法(DPV)测定DA的检出限为8.3 nM。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
求助全文
约1分钟内获得全文 去求助
来源期刊
自引率
0.00%
发文量
0
期刊最新文献
Dye degradation studies on Cu-doped TiO2 thin films developed by reactive sputtering A scrutiny of antibacterial activity of pure and iodine doped ZnO thin films synthesized by mSILAR method Characterization and magnetic phase resolution of CoFe2O4 nanocubes and nanospheres A polyvinyl alcohol/chitosan blend proton exchange membrane for direct methanol fuel cell Improvement of critical parameters of YBCO superconductor by addition of graphene oxide
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1