the influence of the processing parameters on the porosity and microhardness of sintered ti-20nb biomedical alloy

L. Benić, Gorana Domitrović, Žiga Erman, J. Šubić
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Abstract

Titanium based alloys are increasingly used in biomedicine due to their favourable properties. However, because of their high cost, new methods are being developed to produce more economical alloys. Therefore, in the framework of this work, Ti-20Nb alloy was produced by powder metallurgy. Namely, experimental alloy was prepared by mechanical alloying in a ball mill. The samples were singled out from the powder mixture and pressed on a hydraulic press. Sintering was carried out in a tube furnace in an argon atmosphere. Different processing parameters regarding the time and temperature of sintering were applied. Chemical homogeneity was analysed using the energy-dispersive spectrometry. Porosity was observed using the light microscope and microhardness was determined by Vickers method. The obtained results show that with a small correction of the applied technological parameters, in terms of time extension of mixing/mechanical alloying, it is possible to produce economically Ti-20Nb alloy having the properties suitable for biomedical application by using powder metallurgy technology.
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工艺参数对烧结ti-20nb生物医用合金孔隙率和显微硬度的影响
钛基合金以其优良的性能在生物医学领域得到越来越广泛的应用。然而,由于它们的高成本,人们正在开发新的方法来生产更经济的合金。因此,在本工作的框架内,采用粉末冶金法制备Ti-20Nb合金。即在球磨机上进行机械合金化制备实验合金。样品从粉末混合物中挑选出来,在液压机上进行压制。烧结在管式炉氩气环境中进行。采用了不同的烧结时间和烧结温度等工艺参数。用能量色散光谱法分析其化学均匀性。光镜下观察气孔率,维氏法测定显微硬度。结果表明,在混合/机械合金化时间延长方面,采用粉末冶金技术,只要对应用的工艺参数进行很小的修正,就可以经济地生产出具有适合生物医学应用性能的Ti-20Nb合金。
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