Analisis Kadar Kurkumin pada Herbal Oil Kunyit Ekstrak Virgin Coconut Oil dengan Metode Ultrasonik dan Maserasi

R. Mahmudah, Ufilia Quthrotun Nada, Sakinatul Aulia
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Abstract

Vegetable oil theoretically and experimentally has proven its potential as an alternative solvent in the extraction of natural materials. Turmeric infused with virgin coconut oil (VCO) is a way to take advantage of the active compounds from the herbs and the oil itself. This study aims to determine the ability of the VCO solvent in extracting curcumin compounds from turmeric with the addition of tween 80 surfactants. The extraction method used was maceration at 60℃ and an ultrasonic frequency of 40 kHz for 15 minutes. Thin layer chromatography (TLC) was used for qualitative analysis of each herbal oil extract using chloroform: methanol (95:5) eluent and FTIR spectrophotometer to identify functional groups. The highest curcumin content was found in herbal oil with tween 80 of 2 ml, namely 31 ppm in maceration extraction and 260.7 ppm in ultrasonic extraction. Identification of curcumin functional groups in herbal oils showed absorption patterns of O-H, C=O, aromatic C=C, C-O-C, and C-H.
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植物油在理论上和实验上都证明了它作为天然物质提取的替代溶剂的潜力。姜黄注入初榨椰子油(VCO)是一种利用草药和油本身的活性化合物的方法。本研究旨在确定VCO溶剂在添加80种表面活性剂的情况下,从姜黄中提取姜黄素类化合物的能力。提取方法为60℃浸渍,超声频率40 kHz,浸提15 min。采用三氯甲烷:甲醇(95:5)洗脱液,用薄层色谱(TLC)对各草药油提取物进行定性分析,用FTIR分光光度计鉴定官能团。草药油中姜黄素含量最高,在80 ~ 2 ml之间,即浸渍提取31 ppm,超声波提取260.7 ppm。草药油中姜黄素官能团的吸收模式为O- h、C=O、芳香型C=C、C-O-C和C- h。
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