Penentuan Kondisi Optimum pada Pembuatan Surfaktan Natrium Lignosulfonat dari Tempurung Biji Nyamplung

Beta Cahaya Pertiwi, Fariz Santoso Putra, Sintha Soraya Santi
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Abstract

nSodium Lignosulfonate can be produced by Sulphonation of Nyamplung seed shells (Calophyllum inophyllum Linn.) using Sodium Bisulfite as the sulfonating agent. This research was carried out in various operating temperatures of 60 oC, 70 oC, 80 oC, 90 oC, 100 oC and at pH 1,2,3,4,5. Then, the results obtained were analyzed using UV-VIS spectrophotometry. The analysis results that then optimized using the Surface Response Method. The highest levels produced from this study were at a temperature of 100 oC and pH 5 with a concentration of 9.16 mg/L. Optimization is done to determine the optimum conditions for producing Sodium Lignosulfonate. The results of the optimization are known that the optimum conditions are at a temperature of 100 oC and at pH 5 with a concentration of 7.33343 mg/L by using Minitab 18 software. n
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最优化的条件是,从它的外壳中提取利诺硫酸钠
以亚硫酸氢钠为磺化剂,对山龙种壳进行磺化,可制得木质素磺酸钠。本研究在60℃、70℃、80℃、90℃、100℃以及pH为1、2、3、4、5的不同工作温度下进行。然后用紫外-可见分光光度法对所得结果进行分析。利用表面响应法对分析结果进行了优化。在温度为100℃,pH为5,浓度为9.16 mg/L时,本研究产生的最高水平。对生产木质素磺酸钠的最佳工艺条件进行了优化。利用Minitab 18软件进行优化,得到最佳条件为温度100℃,pH 5,浓度7.33343 mg/L
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