Synthesis and characterization of neodymium and nickel particles in polymer base actuator

M. Said, J. Yunas, B. Majlis, B. Bais
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Abstract

A study of synthesization and magnetic properties of cured polymer composite on nickel (Ni) and neodymium (NdFeB) as an actuator membrane to build a micropump for biotechnology instrumentation is prepared in this work. A soft polymeric material such as polydemethilsiloxane (PDMS) and SU8 3050 are used to be mixed with magnetic nanoparticles Ni and NdFeB to produce a composite material. The mixing process is done by using mechanical stirrer with the speed of 1000rpm. In this work, an easy sol-gel method is selected to embed magnetic particles into the polymer matrix. Characterization of particle distribution is observed by metallurgical microscopy and scanning electron microscope (SEM). It is observed that the spreading of magnetic particles inside the polymer chain are constant without clustering effects. Magnetization curves of each sample are traced at room temperature using vibration sample magnetometer (VSM). Good compromising magnetic properties with patternable high aspect ratio structures have been successfully fabricated using a standard MEMS process for an actuator micropump in biomedical application.
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聚合物基致动器中钕镍颗粒的合成与表征
本文研究了以镍(Ni)和钕铁硼(NdFeB)为致动膜的固化聚合物复合材料的合成及其磁性能。采用软质高分子材料聚二甲基硅氧烷(PDMS)和SU8 3050与磁性纳米粒子Ni和NdFeB混合制备复合材料。搅拌过程采用机械搅拌器,转速为1000rpm。在这项工作中,选择了一种简单的溶胶-凝胶方法将磁性颗粒嵌入聚合物基质中。通过金相显微镜和扫描电镜观察了颗粒的分布特征。观察到磁性颗粒在聚合物链内的扩散是恒定的,没有聚类效应。利用振动样品磁强计(VSM)在室温下跟踪各样品的磁化曲线。采用标准的MEMS工艺,成功地为生物医学应用中的致动器微泵制造了具有图像化高纵横比结构的良好妥协磁性能。
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