Study of microstructural formation mechanism of AZ91D magnesium alloy melt during semi-solid isothermal holding

Yuandong Li, Jun-Li Qu, B. Xing, Ying Ma, Tijun Chen
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Abstract

The semi-solid slurry of AZ91D alloy, produced by a novel self-inoculation method, is isothermal treated. Microstructure evolution and mechanism of microstructure formation during isothermal holding are investigated. The results show that primary α-Mg grains are in small size and present polygon morphology in the slurry. During isothermal holding, the size of particles increases with increasing holding time, while the roundness turns better. But the excessive long holding time is bad for the size and roundness of particles. Deformation of dendrite arm is the primary cause of microstructure formation during pouring, meanwhile, ripening and coarsening during isothermal holding. The nucleus generated from the procedure of melt treatment by self-inoculation, and competitive nucleation in undercooled melt which is near the liquidus during isothermal holding is the main source of primary α-Mg phase.
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半固态等温保温AZ91D镁合金熔体组织形成机理研究
采用新型自孕育法制备AZ91D合金半固态浆料,对其进行等温处理。研究了等温保温过程中微观组织的演变及形成机理。结果表明:浆料中α-Mg初生晶粒尺寸较小,呈多边形形态;在等温保温过程中,随着保温时间的延长,颗粒尺寸增大,圆度变好。但保温时间过长,不利于颗粒的尺寸和圆度。枝晶臂的变形是浇注过程中微观组织形成的主要原因,同时也是等温保温过程中成熟和粗化的主要原因。熔体自接种处理过程中产生的核和等温保温过程中接近液相的过冷熔体的竞争形核是初生α-Mg相的主要来源。
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