Effects of Extrusion Processing on the Proximate Compositions of Aerial Yam (Dioscorea bulbifera)-soybean (Glycine max) Flour Blends Using Response Surface Methodology

Enobong O. Umoh, M. Iwe
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Abstract

The impact of extrusion process parameters on the proximate compositions of aerial yam (Dioscorea bulbifera)-soybean (Glycine max) flour blends was investigated with the help of a laboratory scale single-screw extruder, and the flour blending ratio of 25% aerial yam: 75% soybean. Response surface methodology based on Box-Behken design at three factors, five levels of barrel temperature (95, 100, 105, 110, and115℃ ), screw speed (85, 100, 115, 130, and145rpm) and feed moisture (31, 33, 35, 37, and 39%) were used in 20 runs. Adequate and significant (p< 0.05) regression models describing the effects of process parameters on the product quality attributes with high regression coefficient, R2≥  0.9 were obtained, showing that the models can be used to navigate the design space. Results obtained showed that the proximate compositions ranged between 4.03± 0.002 and 5.90± 0.002% ash; 3.10± 0.001 and 7.02± 0.003% moisture content; 2.70± 0.001 and 4.67± 0.003% fibre; 24.57± 0.078 and 36.79± 0.004% protein; 11.39± 0.004 and 35.35± 0.011% lipid. The best extrusion condition combinations were 1150C barrel temperature, 115rpm screw speed and 35% feed moisture for ash content; 1000C barrel temperature, 130rpm screw speed and 33% feed moisture for moisture content; 1150C barrel temperature, 115rpm screw speed and 35% feed moisture for fibre content; 1050C barrel temperature, 145rpm screw speed and 35% feed moisture for protein content; 1050C barrel temperature, 85rpm screw speed and 35% feed moisture for lipids. Analysis of variance showed that only barrel temperature affected the ash composition significantly (p< 0.05). Barrel temperature, screw speed and feed moisture showed insignificant (p> 0.05) effect on moisture content, while fibre content was significantly (p< 0.05) affected by barrel temperature and screw speed. Protein and crude fat (lipid) contents were significantly (p< 0.05) affected by barrel temperature, screw speed and feed moisture.
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利用响应面法研究挤压加工对地药-大豆混合粉近似成分的影响
采用实验室规模的单螺杆挤出机,考察了挤出工艺参数对地瓜粉与大豆粉混料近似成分的影响,确定了地瓜粉与大豆粉的混料比例为25%:75%。基于Box-Behken设计的响应面方法在三个因素下进行了20次运行,即5个水平的桶温(95、100、105、110和115℃)、螺杆转速(85、100、115、130和145rpm)和进料水分(31、33、35、37和39%)。得到了充分且显著(p< 0.05)的描述工艺参数对产品质量属性影响的回归模型,回归系数高,R2≥0.9,表明该模型可用于导航设计空间。结果表明:灰分的近似组成在4.03±0.002 ~ 5.90±0.002%之间;3.10±0.001和7.02±0.003%含水率;2.70±0.001和4.67±0.003%纤维;24.57±0.078和36.79±0.004%蛋白;11.39±0.004和35.35±0.011%脂质。最佳挤出条件组合为料筒温度1150C,螺杆转速115rpm,进料水分35%;桶温1000C,螺杆转速130rpm,给料水分33%为含水率;1150C的桶温,115rpm的螺杆转速和35%的饲料水分用于纤维含量;1050C的桶温,145rpm的螺杆转速,35%的饲料水分用于蛋白质含量;1050℃的桶温,85转/分钟的螺杆转速,35%的进料水分用于脂质。方差分析表明,只有桶温对灰分组成有显著影响(p< 0.05)。料筒温度、螺杆转速和饲料含水量对水分含量的影响不显著(p> 0.05),而纤维含量受料筒温度和螺杆转速的影响显著(p< 0.05)。蛋白质和粗脂肪含量受料筒温度、螺杆转速和饲料水分影响显著(p< 0.05)。
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