The Performance of Micro-Fabricated Gas Chromatographic Columns with Different Number of Serpentine Turns

Qiyong Liuo, Fei Feng, Xuelei Yang, Bin Zhao, Yangyang Zhao, Haimei Zhou, Guiyang Zhang, Xinxin Li
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引用次数: 1

Abstract

In this paper, the separation performance of two kinds of micro-fabricated gas chromatographic columns ($\mu\mathrm{GC}$-columns) with different numbers of serpentine turns, respectively 51 and 101, had been studied. These two kinds of $\mu\mathrm{GC}$-columns had the same inner structure, column length and stationary phase (alumina). The test results of C10 demonstrated that the $\mu \mathrm{GC}$-column with 51 serpentine turns had better the numbers of theoretical plates and shorter separation time compared with the 101 serpentine turns. Particularly, the improvement of number of theoretical plates of C10 could reach up to 251% at under 22.2 kPa inlet pressure, which contributed to less “race track effect” caused by less serpentine turns.
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不同蛇形匝数的微制气相色谱柱的性能
本文研究了两种不同蛇形匝数(51和101)的微型制备气相色谱柱($\mu\ mathm {GC}$-柱)的分离性能。这两种$\mu\mathrm{GC}$-色谱柱的内部结构、柱长和固定相(氧化铝)相同。C10的试验结果表明,51个蛇形匝数的$\mu \mathrm{GC}$-柱比101个蛇形匝数的柱具有更好的理论板数和更短的分离时间。特别是在22.2 kPa进口压力下,C10的理论板数提高了251%,减少了蛇形弯道带来的“赛道效应”。
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