ANALYSIS OF TOTAL NITROGEN LEVELS IN SOLID FERTILIZER WITH KJEDAHL METHOD IN BALAI PENGKAJIAN TEKNOLOGI PERTANIAN (BPTP) YOGYAKARTA

F. I. Fajarwati, Athalia Tasya Hermawati, Sri Widada
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Abstract

An analysis of the determination of N-Total levels in fertilizer has been carried out at the Yogyakarta Agricultural Technology Assessment Center (BPTP). This study aims to determine the total nitrogen content in the fertilizer sample. Analysis of nitrogen content in fertilizers was carried out using the Kjeldahl method. The principle of determining total nitrogen using the Kjeldahl method is that nitrogen in fertilizer samples is hydrolyzed with concentrated sulfuric acid to form ammonium sulfate compounds. The product of the destruction is ammonium sulfate compound which is distilled in an alkaline condition which is then accommodated with boric acid. The resulting distillate is titrated with sulfuric acid solution until a green color changes to pink. From the results of the levels of N-Total obtained in the sample PO.207 with N-Total 1.8136%, PO.208 with N-Total 1.5597%, PO.209 with N-Total 1.5489%, PO.210 with N-Total 1.385%, PO.211 with N-Total 1.1292% and PO.212 with N-Total 2.2401%.
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日惹balai pengkajian technologipertanian (bptp)固体肥料中总氮含量的kjedahl法分析
日惹农业技术评估中心(BPTP)对肥料中总氮水平的测定进行了分析。本研究旨在测定肥料样品中的总氮含量。采用凯氏定氮法对肥料中氮含量进行了分析。凯氏定氮法测定总氮的原理是用浓硫酸水解肥料样品中的氮,生成硫酸铵化合物。破坏的产物是硫酸铵化合物,在碱性条件下蒸馏,然后与硼酸调和。所得馏出物用硫酸溶液滴定,直到绿色变为粉红色。样品PO.207 N-Total含量为1.8136%,PO.208 N-Total含量为1.5597%,PO.209 N-Total含量为1.5489%,PO.210 N-Total含量为1.385%,PO.211 N-Total含量为1.1292%,PO.212 N-Total含量为2.2401%。
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