A Comparative Study of pH Changes, Releasing Elements and solubility of Bioceramic Sealers.

B. Rathod
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Abstract

Abstract: Introduction: Bioceramic technology has been introduced recently in endodontics to benefit from the hydroxyapatite formation during the setting reaction in the presence of tissue fluid and establish a chemical bond at the dentin interface. Aim: To compare the physiochemical properties (pH changes, releasing elements and solubility) of different newer Bioceramic sealer (Ceraseal) with mineral trioxide aggregate (MTA-Fillapex) sealers. Material and Method: Samples were prepared by using three different injectable sealer placed in 20 ring moulds, 10 of each sealer. Each sample was prepared with an internal diameter of 10 mm and a height of 3mm. The samples were digitally weighed to register the mass of each specimen before and after immersion in distilled water. The pH value was measured by a digital pH meter, releasing elements measured in atomic absorption spectrophotometer, and solubility measured in digital weighed machine. After 1, 7, 14 and 28 days, pH changes, released elements and solubility was the data obtained calculated and statistically analysed. Results: Ceraseal Sealer exhibited high alkaline pH over time and also showed significantly higher solubility (P < 0.05). Conclusion: Bioceramic sealer shows more alkalinity and calcium ion release compared to the MTA sealer. The alkalinity nature of the bioceramic sealer, corresponds to the increase in solubility. So bioceramic sealer are more alkaline, calcium releasing and soluble.  
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生物陶瓷封口剂pH值变化、释放元素及溶解度的比较研究。
摘要:生物陶瓷技术最近被引入到牙髓学中,利用在组织液存在下的固化反应过程中羟基磷灰石的形成,并在牙本质界面建立化学键。目的:比较不同新型生物陶瓷封口剂(Ceraseal)与三氧化二矿骨料封口剂(MTA-Fillapex)的理化性质(pH值变化、释放元素及溶解度)。材料和方法:将三种不同的注射密封剂放置在20个环形模具中制备样品,每种密封剂10个。每个样品的内径为10 mm,高度为3mm。对样品进行数字称重,以记录浸泡在蒸馏水之前和之后的每个样品的质量。用数字pH计测定pH值,用原子吸收分光光度计测定释放元素,用数字称重机测定溶解度。计算1、7、14、28 d后的pH变化、释放元素和溶解度数据,并进行统计分析。结果:随着时间的推移,Ceraseal Sealer呈现出较高的碱性pH值,且溶解度显著提高(P < 0.05)。结论:生物陶瓷封口剂比MTA封口剂具有更高的碱性和钙离子释放量。生物陶瓷密封剂的碱性,对应于溶解度的增加。所以生物陶瓷封口剂碱性强,释钙性强,易溶性好。
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