The Production of Biodiesel from Sewage Sludge Via Soxlet Extraction Using Hexane and Ethyl Acetate in Ratio 2:1 As the Organic Solvent and Transesterification Reaction

W. Ivwurie, B. Okoro
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Abstract

The Lipid/oil was extracted from reduced dried primary sewage sludge particle using soxhlet extraction method with Hexane and Ethyl Acetate in the ratio 2:1 as the extracting solvent. The extracted oil gave 15.03% percentage yield with density of 0.845 g/ml, pH value of 8.97, specific gravity of 0.845, viscosity of 41.20 mm2/sec, kinematic viscosity of 42.18 mm2/sec. The lipid/oil was brownish black in colour with a pungent smell. The chemical analyses revealed saponification value of 168.00 mgKOH/g, acid value of 5.60 mgKOH/g and free fatty acid value of 2.80%. The physicochemical analyses of the biodiesel produced gave a c percentage yield of 40% biodiesel, density of 0.845 Kg/ml, pH value of 8.50, specific gravity of 0.845, kinematic viscosity of 4.80 mm2/s, acid value of 0.37 mg KOH/g, and flash point of 150°C, cloud point of 5°C and pour point of -2°C. The results of the physicochemical parameters from the research shows that the feedstock (primary sewage sludge) would be a good source for the production of biodiesel. Original Research Article Ivwurie and Okoro; JABB, 23(6): 43-47, 2020; Article no.JABB.60976 44
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以正己烷和乙酸乙酯为有机溶剂,以索氏萃取法从污水污泥中提取生物柴油,并进行酯交换反应
采用索氏萃取法,以己烷与乙酸乙酯的比例为2:1,从还原干燥的污水初级污泥颗粒中提取油脂。萃取油得率为15.03%,萃取油密度为0.845 g/ml, pH值为8.97,比重为0.845,粘度为41.20 mm2/sec,运动粘度为42.18 mm2/sec。脂质/油呈棕黑色,有刺鼻的气味。化学分析显示皂化值为168.00 mgKOH/g,酸值为5.60 mgKOH/g,游离脂肪酸值为2.80%。经理化分析,所得生物柴油产率为40%,密度为0.845 Kg/ml, pH值为8.50,比重为0.845,运动粘度为4.80 mm2/s,酸值为0.37 mg KOH/g,闪点为150°c,浊点为5°c,倾点为-2°c。研究的理化参数结果表明,该原料(初生污泥)是生产生物柴油的良好原料。Ivwurie和Okoro;Jabb, 23(6): 43-47, 2020;文章no.JABB。60976年44
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