Hot deformation and fatigue behaviour of a zinc base doped biocompatible material: characterization of plasma spray coating on surface

IF 2 3区 材料科学 Q2 ENGINEERING, MECHANICAL Surface Topography: Metrology and Properties Pub Date : 2023-08-21 DOI:10.1088/2051-672X/acf234
V. B, Suresh Sonagiri, S. S
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Abstract

Composite materials are natural or man-made substances put into the body to turn a living cell into a working organ. Bone tissue and biocompatibility are emerging as an alternative approach to regenerating bone due to some distinct advantages over autografting. This research aimed to fabricate a novel porous scaffold that can be utilized as a bone substitute. Zn-nHApx-Srx (x = 0, 3, 6, 9) was selected by different weight ratios and synthesized using the powder metallurgy method. The utilization of nanohydroxyapatite (Ca10(PO4)6(OH)2) is due to its excellent biocompatibility with the human body. Polylactic-co-glycolic acid (PLGA) is incorporated to get enhanced biological performance. Plasma spray coating was performed on a zinc substrate using pure and doped biocomposites calcined at 800 °C. The biocomposites tensile strength increased between 0.4 and 19.8 MPa by increasing Zn and Sr weight ratios. In addition, 3% Sr/2.5% Zn with 2% of nHAp-PLGA composite showed improved hardness, which is beneficial for resembling bone tissue and die-casting fittings in automobile manufacturing applications. Mechanical properties, FT-IR, hot deformation behaviour, and SEM techniques help us understand the behaviour of Zn-Sr-nHAp in a vial containing PLGA. The highest ultimate tensile strength of 182 MPa and improved flow softening behaviour are achieved in a coated Zn/6% (nHAp-Sr) mixture suitable for biodegradable implant applications.
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锌基掺杂生物相容性材料的热变形和疲劳行为:表面等离子喷涂涂层的表征
复合材料是一种天然的或人造的物质,用于将活细胞转化为工作器官。由于骨组织和生物相容性比自体移植有一些明显的优势,因此正在成为再生骨的替代方法。本研究旨在制造一种新型多孔支架,可作为骨替代物。选择不同重量比的zn - nhax - srx (x = 0,3,6,9),采用粉末冶金法合成。纳米羟基磷灰石(Ca10(PO4)6(OH)2)的利用是由于其与人体良好的生物相容性。加入聚乳酸-羟基乙酸(PLGA)以提高生物性能。在800°C下煅烧的纯和掺杂生物复合材料在锌基体上进行等离子喷涂。随着Zn和Sr质量比的增加,生物复合材料的抗拉强度提高了0.4 ~ 19.8 MPa。此外,3% Sr/2.5% Zn和2% nHAp-PLGA复合材料的硬度有所提高,有利于类似骨组织和压铸件在汽车制造中的应用。机械性能,FT-IR,热变形行为和SEM技术帮助我们了解Zn-Sr-nHAp在含有PLGA的小瓶中的行为。在适用于生物可降解植入物的涂覆Zn/6% (nHAp-Sr)混合物中,达到了182 MPa的最高极限拉伸强度和改善的流动软化行为。
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来源期刊
Surface Topography: Metrology and Properties
Surface Topography: Metrology and Properties Materials Science-Materials Chemistry
CiteScore
4.10
自引率
22.20%
发文量
183
期刊介绍: An international forum for academics, industrialists and engineers to publish the latest research in surface topography measurement and characterisation, instrumentation development and the properties of surfaces.
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