Radish (Raphanus sativus) Leaves Mediated CuO-NiO Nanocomposite for Photocatalytic Activity

V. Pavitra, H. Divya, B. Praveen, G. Nagaraju, Udayabhanu
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引用次数: 1

Abstract

Fundamental and applied research depends on the removal of organic toxic effluents from textile industries. Photocatalytic dye degradation of CuO-NiO nanocomposite has been studied against methylene blue (MB) dye. CuO-NiO nanocomposite has been prepared by hydrothermal method using radish (Raphanus sativus) leaves as green fuel. Prepared composite nanoparticles (NPs) are characterized by XRD, FTIR, UV-DRS and SEM with EDS for the elemental and structural information. XRD data indicated the formation of monoclinic and hexagonal crystallite structures for CuO and NiO respectively. FTIR confirmed the presence of Cu - O and Ni - O molecular vibrations. Surface morphology and elemental composition of composite was analysed by SEM with EDS. CuO-NiO nanocomposite is capable to degrade 70 % of methylene blue (MB) dye in 180 min under UV light interactions. Recyclability is also good even after 4 cycles of degradation experiment for the CuO-NiO composite.
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萝卜叶片介导的CuO-NiO纳米复合材料的光催化活性研究
基础和应用研究依赖于去除纺织工业的有机有毒废水。研究了CuO-NiO纳米复合材料在亚甲基蓝(MB)染料上的光催化降解染料。以萝卜叶为绿色燃料,采用水热法制备了CuO-NiO纳米复合材料。采用XRD、FTIR、UV-DRS和SEM对制备的复合纳米粒子进行了表征,并用能谱仪分析了纳米粒子的元素和结构信息。XRD数据表明,CuO和NiO分别形成单斜晶和六方晶结构。FTIR证实了Cu - O和Ni - O分子振动的存在。利用扫描电镜和能谱仪分析了复合材料的表面形貌和元素组成。在紫外光作用下,CuO-NiO纳米复合材料可在180 min内降解70%的亚甲基蓝(MB)染料。经过4次循环降解实验,CuO-NiO复合材料的可回收性也很好。
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