Focused Ion Beam Assisted Etching of Aluminum.

F. Itoh, Junzo Azuma, S. Haraichi, A. Shimase
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Abstract

Focused ion beam (FIB) milling is widely used for circuit repair, mask repair, and SEM sample prepair for cross-section observation. In the circuit repair application, it is important to achive a higher material selectivity of Al/SiO2, and a higher milling rate. In order to realize both of these, focused ion beam assisted etching (FIBAE), where a chlorine containing gas is injected towards the milling site, was performed. Using Cl2 gas only caused a significant side etch, though the etching rate of aluminum was quite high. When etching Al-Cu-Si alloy with a chlorine containing gas, a residue of Cu-Cl compound was formed. This can be decreased by heating the sample as high as 200°C. An etching selectivity (Al/SiO2) of 100 was achived, without side-etching, by a gas mixture of SiCl4 (95%) and Cl2 (5%).
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聚焦离子束辅助蚀刻铝。
聚焦离子束(FIB)铣削广泛应用于电路修复、掩模修复和SEM样品制备的截面观察。在电路修复应用中,实现更高的Al/SiO2材料选择性和更高的铣削速率是重要的。为了实现这两个目标,进行了聚焦离子束辅助蚀刻(FIBAE),其中向铣削部位注入含氯气体。使用Cl2气体只引起明显的侧蚀刻,尽管铝的蚀刻率相当高。在含氯气体中蚀刻铝铜硅合金时,会形成残留的Cu-Cl化合物。这可以通过将样品加热到高达200°C来降低。在SiCl4(95%)和Cl2(5%)的混合气体中,在没有侧刻的情况下,Al/SiO2的选择性为100。
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