3D Confocal Imaging Methodology Optimized for Pore Space Characterization of Microporous Carbonate Reservoirs

A. Hassan, V. Chandra, M. Yutkin, T. Patzek
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Abstract

Microporous carbonates host a significant portion of the remaining oil-in-place in the giant carbonate reservoirs of the Middle East. Carbonates host wide range of pore sizes, however the key element influencing hydrocarbon flow is pore interconnectivity. We evaluate the use of confocal microscopy to image fluorescent epoxy pore casts of microporous carbonates. The acquired high-resolution 3D confocal images are used to gain invaluable insights on the interconnectivity between macroporosity and microporosity. We analyzed the sensitivity of quality of epoxy pore cast images to: fluorochrome selection, objective lens, and imaging medium by imaging standard fluorescent spherical beads. Guided by the sensitivity results, we acquired 3D images of the multi-modal pore space in an Indiana limestone sample with lateral- and axial-resolution of 0.36 µm and 2 µm, respectively. And we were able to identify the multi-scale pore types in the studied carbonate sample and highlight their interconnectivity.
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微孔碳酸盐储层孔隙空间表征优化的三维共聚焦成像方法
在中东地区的巨型碳酸盐岩储层中,微孔碳酸盐岩占有相当大一部分的剩余油。碳酸盐岩储集孔径范围广,但影响油气流动的关键因素是孔隙连通性。我们评估使用共聚焦显微镜成像荧光环氧树脂微孔碳酸盐的孔铸件。获得的高分辨率3D共聚焦图像用于获得关于宏观孔隙和微观孔隙之间相互联系的宝贵见解。通过成像标准荧光球珠分析了环氧孔铸像质量对荧光染料选择、物镜和成像介质的敏感性。在灵敏度结果的指导下,我们获得了印第安纳石灰岩样品中多模态孔隙空间的三维图像,其横向和轴向分辨率分别为0.36µm和2µm。在研究的碳酸盐样品中,我们能够识别出多尺度孔隙类型,并突出了它们之间的连通性。
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