Preparation and Characterization of Mustard Stalks Derived Carboxymethyl Cellulose and Poly(L-Lactic Acid) Biocomposites

Md. Hafezur Rahaman, Mahfuja Rahman, S. Alam, M. Sultana, M. S. Parvez, Asadullah Ahmed
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引用次数: 3

Abstract

The influences of poly ( L- lactic acid) (PLLA) and carboxymethyl cellulose (CMC) derived from mustard stalks content on the morphological and thermal properties of PLLA/CMC biocomposites were investigated. The yield of CMC from microcrystalline cellulose (MCC) of mustard stalks was about 78%. Biocomposites were prepared using the solution casting method, varying PLLA, and CMC ratio. Prepared samples were characterized using Fourier transform infrared (FTIR) spectroscopy, differential scanning calorimetric, X-ray diffraction, and scanning electron microscopy. The decomposition temperature of CMC was increased and formed excellent biocomposites with PLLA. Composite crystallinity was varied with the percentages of the CMC. The CMC fibers coated with a layer of PLLA suggested that CMC and PLLA have good compatibility.
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芥菜茎源羧甲基纤维素与聚l -乳酸生物复合材料的制备与表征
研究了聚L-乳酸(PLLA)和芥菜茎源羧甲基纤维素(CMC)含量对聚L-乳酸/羧甲基纤维素生物复合材料形态和热性能的影响。以芥菜茎微晶纤维素(MCC)为原料制备CMC的收率约为78%。采用溶液浇铸法,改变PLLA和CMC的比例制备生物复合材料。利用傅里叶变换红外光谱、差示扫描量热、x射线衍射和扫描电镜对制备的样品进行了表征。提高了CMC的分解温度,与PLLA形成了优良的生物复合材料。复合结晶度随CMC含量的变化而变化。CMC纤维包覆一层PLLA,表明CMC与PLLA具有良好的相容性。
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