Evolution of Structure and Properties of Nickel-Enriched Ti-Ni Shape Memory Alloy subjected to Compressive Deformation

V. Komarov, I. Khmelevskaya, R. Karelin, V. Yusupov, I. Postnikov, G. Korpała, R. Kawalla, U. Prahl, S. Prokoshkin
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Abstract

The effect of compressive deformation of the nickel-enriched Ti-Ni shape memory alloy in a temperature range of 100 to 900 °С on phase composition, microstructure, mechanical and functional properties was studied. The temperature ranges of dynamic recovery, polygonization and recrystallization were determined as a result of comparative optical microscopy, XRD, DSC studies, HV measurements and shape recovery testing. Lowering of the compressive deformation temperature is accompanied by an increase in a hardness value from 280 to 350 HV and leads to decrease in average grain size from 33 to 16 μm. The dispersion hardening leads to an increase in shape recovery properties. The optimum deformation temperature range for thermomechanical treatment of Ti-Ni SMA from the viewpoint of ultrafine-grained structure and high functional properties formation was determined as 400 to 600 °C.
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压缩变形下富镍Ti-Ni形状记忆合金的组织与性能演变
研究了富镍Ti-Ni形状记忆合金在100 ~ 900°С温度范围内压缩变形对合金相组成、显微组织、力学性能和功能性能的影响。通过对比光学显微镜、XRD、DSC研究、HV测量和形状恢复测试,确定了动态恢复、多角化和再结晶的温度范围。压缩变形温度降低,合金硬度从280 ~ 350 HV升高,平均晶粒尺寸从33 μm减小到16 μm。分散硬化导致了形状恢复性能的提高。从形成超细晶组织和高功能性能的角度出发,确定了Ti-Ni SMA热处理的最佳变形温度范围为400 ~ 600℃。
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