Features of the impact of hot isostatic pressing and heat treatment on the structure and properties of maraging steel obtained by selective laser melting method

A. O. Kayasova, E. Levashov
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Abstract

Using the SLM method in a nitrogen blanket with heating to a temperature of 200 °C, samples were obtained at a position of 0° against the build plate. The effect of the hot isostatic pressing (HIP) and heat treatment (HT: hardening + aging) on the structure and mechanical properties of maraging steel CL50 WS was studied (the Russian analogue is ChS4 grade). To analyze the effect of post-processing on the strength characteristics (σb, σ0,2, δ, ψ), tensile tests were conducted. Their results indicated high values of strength and ductility. It has been established that as a result of HT in the steel structure, in addition to α-Fe, γ-Fe, dispersed precipitates of the NiTi3 strengthening phase are formed, the identification of which was carried out by high-resolution transmission electron microscopy. Through the NiTi3 intermetallic phase, the steel has acquired increased tensile strength and yield strength required for the production of critical components and parts for highly loaded turbomachine disks. The change in the porosity of the samples before and after the HIP was analyzed. The microstructure of the samples and the changes that occur under the influence of various post-processing options are studied. The fine-grained homogeneous structure obtained by combining the SLM, HIP and HT provided optimal strength and ductility. Analysis of fractures after mechanical testing showed that the samples after postprocessing are destroyed according to the viscous-pitting mechanism with the formation of a neck.
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热等静压和热处理对选择性激光熔化法马氏体时效钢组织和性能影响的特点
采用SLM方法,在氮气毯中加热至200℃,在与构建板0°的位置获得样品。研究了热等静压(HIP)和热处理(HT:硬化+时效)对马氏体时效钢CL50 WS(俄罗斯类似物为ChS4级)组织和力学性能的影响。为了分析后处理对强度特性(σb, σ0,2, δ, ψ)的影响,进行了拉伸试验。他们的结果表明,高值的强度和延展性。结果表明,高温作用在钢组织中,除了α-Fe、γ-Fe外,还形成了NiTi3强化相的分散析出相,并通过高分辨率透射电镜进行了鉴定。通过NiTi3金属间相,该钢获得了更高的抗拉强度和屈服强度,用于生产高负荷涡轮机械盘的关键部件和零件。分析了热处理前后试样孔隙率的变化。研究了样品的微观结构以及在各种后处理方案的影响下发生的变化。结合SLM、HIP和HT获得的细晶均匀组织提供了最佳的强度和延展性。力学试验后的断口分析表明,后处理后的试样按粘点破坏机制破坏,并形成颈状。
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