Preparation and Characterization of Polyaniline-Co 3 O 4 Nanocomposites via Interfacial Polymerization

M. Bedre, R. Deshpande, Basavaraja Salimath, V. Abbaraju
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引用次数: 41

Abstract

Polyaniline (Pani) and Polyaniline-Co3O4 nanocomposites (PCO) were prepared by employing interfacial po- lymerization using ammonium persulphate as an oxidizing agent. The formations of regular nanocomposite materials were studied by Fourier transform infrared (FTIR) spectroscopy and XRD techniques. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) images were conducted to characterize the morphology. Thermo-gravimetric (TG) and differential thermal analysis (DTA) were carried out study the thermal stability of the resulting composites. The nano- composites were weakly ferromagnetic at room temperature. Formation of conducting emeraldine salt form was concluded by electrical conductivity.
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界面聚合法制备聚苯胺-氧化钴纳米复合材料及其表征
以过硫酸铵为氧化剂,采用界面聚合法制备了聚苯胺(Pani)和聚苯胺- co3o4纳米复合材料。利用傅里叶变换红外光谱(FTIR)和x射线衍射(XRD)技术研究了规则纳米复合材料的形成。采用扫描电镜(SEM)和透射电镜(TEM)对其形貌进行表征。通过热重分析(TG)和差热分析(DTA)研究了复合材料的热稳定性。纳米复合材料在室温下具有弱铁磁性。通过电导率分析,得出了导电绿宝石盐形态的形成。
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