Spinel-Type Cobalt Oxide Nanoparticles: Synthesis, Characterization and Antibacterial Properties

S. Ambika, S. Gopinath, K. Sivakumar, K. Saravanan
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Abstract

A series of cobalt oxide nanoparticles (sample A (300 °C), sample B (400 °C) and sample C (500 °C)) are synthesized in a starch medium by the hydrothermal method followed by annealing. The structural, morphological, and magnetic, of these cobalt oxide nanoparticles, become characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), vibrating sample magnetometer (VSM) correspondingly. Furthermore, it can be seen that the increase in the synthesis temperature results in a substantial increase in the average particle size. The impact of synthesis temperature in relation to morphology (size and shape) and magnetic properties of cobalt oxide nanoparticles has been investigated. Besides, the antibacterial and catalytic activity of these nanoparticles are examined. A systematic analysis is presented on the influence of parameters of synthesis on the formation and structural properties of cobalt oxide nanoparticles. We expect in which this topic will give many valuable ideas for the metal oxide nanomaterials development, synthesis, as well as applications.
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尖晶石型氧化钴纳米颗粒:合成、表征及抗菌性能
采用水热法在淀粉介质中合成了一系列氧化钴纳米颗粒(样品A(300℃),样品B(400℃)和样品C(500℃)),然后进行退火。通过x射线衍射(XRD)、扫描电子显微镜(SEM)、透射电子显微镜(TEM)、振动样品磁强计(VSM)等手段对氧化钴纳米颗粒的结构、形态和磁性进行了表征。此外,可以看出,合成温度的升高导致平均粒径的大幅增加。研究了合成温度对氧化钴纳米颗粒形貌(尺寸和形状)和磁性能的影响。此外,还测试了这些纳米颗粒的抗菌和催化活性。系统分析了合成工艺参数对氧化钴纳米颗粒的形成和结构性能的影响。本课题将为金属氧化物纳米材料的开发、合成和应用提供一些有价值的思路。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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