S. R. Bireddy, Venkata Ramana Reddy Chittireddy, L. Eppakayala
{"title":"PEG-600: Greensolvent for synthesis of pyrazolo[5,1-c]thieno[3,4-e][1,2,4]triazin-6-amine","authors":"S. R. Bireddy, Venkata Ramana Reddy Chittireddy, L. Eppakayala","doi":"10.1063/5.0060858","DOIUrl":null,"url":null,"abstract":"Using polyethylene glycol (PEG-600) as a reaction medium for the synthesis of 3, the green, onepot, multicomponent method was developed. Tandem-prepared compound 3 with excellent yields, without isolation of intermediates in situ. Thus, using PEG-600 as a solvent, novel Pyrazolo[5,1-c]thieno[3,4e][1,2,4]triazine-6-amine(3) products have been prepared with new synthetic routes and techniques.","PeriodicalId":18837,"journal":{"name":"NATIONAL CONFERENCE ON PHYSICS AND CHEMISTRY OF MATERIALS: NCPCM2020","volume":"72 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2021-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"NATIONAL CONFERENCE ON PHYSICS AND CHEMISTRY OF MATERIALS: NCPCM2020","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1063/5.0060858","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
Abstract
Using polyethylene glycol (PEG-600) as a reaction medium for the synthesis of 3, the green, onepot, multicomponent method was developed. Tandem-prepared compound 3 with excellent yields, without isolation of intermediates in situ. Thus, using PEG-600 as a solvent, novel Pyrazolo[5,1-c]thieno[3,4e][1,2,4]triazine-6-amine(3) products have been prepared with new synthetic routes and techniques.