Production Process of Large Pore Size Activated Carbon from Palm Kernel Shell using Sodium Chloride as An Activator

Ahmad Nurdin, I. Iriani, H. Harahap, A. Fahmi
{"title":"Production Process of Large Pore Size Activated Carbon from Palm Kernel Shell using Sodium Chloride as An Activator","authors":"Ahmad Nurdin, I. Iriani, H. Harahap, A. Fahmi","doi":"10.30598/ijcr.2022.10-ahm","DOIUrl":null,"url":null,"abstract":"This study aimed to determine the yield of activated carbon, iodine number, and surface area of palm activated carbon. Samples were produced by using sodium chloride (NaCl) as an activator. Palm shells that had been produced by the milling process were then sieved with a 12 mesh sieve and soaked in 20 % NaCl solution. The sample solution was heated over a water bath at 70 oC and continued with the drying process at a constant temperature of 105 oC. The activated shells continued the pyrolysis process at temperatures of 300, 400, and 500 oC for 3 hours. The activated carbon obtained from the pyrolysis process was weighed and then washed using hot distilled water. The samples were dried in an oven at a temperature of 105 oC for 24 hours. The results were analyzed for iodine number using iodometric titration method, surface area using Brunauer- Emmett-Teller (BET) method, and pore structure using the Scanning Electron Microscope (SEM) method. The results showed the best yield was 38.13 % obtained at 20% NaCl and a temperature of 400 oC. The best iodine number was 767.745 mg/g and surface area was 6.790 m2/g, pore volume 4.377 cc/g with pore size 9.781 A.","PeriodicalId":13392,"journal":{"name":"Indo. J. Chem. Res.","volume":"44 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2022-05-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Indo. J. Chem. Res.","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.30598/ijcr.2022.10-ahm","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

Abstract

This study aimed to determine the yield of activated carbon, iodine number, and surface area of palm activated carbon. Samples were produced by using sodium chloride (NaCl) as an activator. Palm shells that had been produced by the milling process were then sieved with a 12 mesh sieve and soaked in 20 % NaCl solution. The sample solution was heated over a water bath at 70 oC and continued with the drying process at a constant temperature of 105 oC. The activated shells continued the pyrolysis process at temperatures of 300, 400, and 500 oC for 3 hours. The activated carbon obtained from the pyrolysis process was weighed and then washed using hot distilled water. The samples were dried in an oven at a temperature of 105 oC for 24 hours. The results were analyzed for iodine number using iodometric titration method, surface area using Brunauer- Emmett-Teller (BET) method, and pore structure using the Scanning Electron Microscope (SEM) method. The results showed the best yield was 38.13 % obtained at 20% NaCl and a temperature of 400 oC. The best iodine number was 767.745 mg/g and surface area was 6.790 m2/g, pore volume 4.377 cc/g with pore size 9.781 A.
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
以氯化钠为活化剂制备棕榈仁壳大孔径活性炭的工艺研究
本研究旨在确定活性炭的产率、碘值和棕榈活性炭的表面积。以氯化钠(NaCl)为活化剂制备样品。研磨后的棕榈壳用12目筛筛过,浸泡在20% NaCl溶液中。样品溶液在70℃的水浴中加热,并在105℃的恒温下继续干燥过程。活化后的壳在300、400和500℃的温度下继续热解3小时。将热解得到的活性炭称重,然后用热蒸馏水洗涤。样品在105℃的烘箱中干燥24小时。用碘滴定法分析了样品的碘值,用bruauer - emmet - teller (BET)法分析了样品的表面积,用扫描电镜(SEM)法分析了样品的孔隙结构。结果表明,在NaCl浓度为20%、温度为400℃的条件下,产率最高为38.13%。最佳碘值为767.745 mg/g,比表面积为6.790 m2/g,孔体积为4.377 cc/g,孔径为9.781 A。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
求助全文
约1分钟内获得全文 去求助
来源期刊
自引率
0.00%
发文量
0
期刊最新文献
Study Effect of Chitosan-Epichlorohydrin Macropore Beads on Decreasing the Value of Total Dissolved Solid (TDS) and Dyes in Sasirangan Liquid Waste Treatment Synthesis and Characterization of Silica Gel from Palm Shell and Coir Ash Study of Anthocyanin Molecule Blocking as Anti-Hypertensive through the Pathway of the Renin-Angiotensin-Aldosterone System (RAAS) Antioxidant Activity of Ethanol and n-hexane Extracts of Javanese Bark (Lannea coromandelica) Using the DPPH Method Synthesis and Characterization of Silver Nanoparticles from the Leaf Stalk Extract of Moringa oleifera
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1