The microanalysis of copper-coated diamond composite powders prepared by electroless plating

Lianmeng Zhang, Shuya Xiong, Ruxia Liu, Jian Zhang, G. Luo, Q. Shen
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引用次数: 1

Abstract

Diamond-Cu matrix composite with high thermal conductivity and low coefficient of thermal expansion has been the high-performance thermal management materials. High-performance copper-coated diamond composite powders were successfully prepared using electroless plating at an appropriate bath temperature, pH value, copper ions concentration. The XRD results showed the coated Cu was highly pure with very little oxygen content. The SEM results that the particle size and surface roughness increased, with the increase of bath temperature, pH value, copper ions concentration separately. Finally, diamond-Cu composite powers with dense Cu coating and homogeneous Cu particles could be obtained under the optimum process conditions at the reaction temperature of 45 °C, pH value of 12.5 and copper ions concentration of 0.10 mol/L.
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化学镀镀铜包覆金刚石复合粉末的显微分析
金刚石- cu基复合材料具有高导热系数和低热膨胀系数,是一种高性能的热管理材料。在适当的镀液温度、pH值、铜离子浓度条件下,采用化学镀法制备了高性能铜包覆金刚石复合粉体。XRD结果表明,包覆的Cu纯度高,氧含量极低。SEM结果表明,随着镀液温度、pH值、铜离子浓度的升高,颗粒尺寸增大,表面粗糙度增大。在反应温度为45℃、pH值为12.5、铜离子浓度为0.10 mol/L的最佳工艺条件下,可制得Cu包覆致密、Cu颗粒均匀的金刚石-Cu复合粉体。
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