Effect of Deformation on the Mechanical Properties of Sn-5wt%Sb Alloy

Sadiq H. Khoreem, A. Meftah, T. T. Alnahari
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Abstract

Sn–5wt%Sb is one of the materials considered for replacing Pb-bearing alloys in electronic packaging. The mechanical response of Sn–5wt% Sb solder alloy has been tested under different strain rates and three deformation temperatures. The behavior of true strain–time of Sn–5wt% Sb solder alloy has been investigated over strain rates of and deformation temperatures of 313, 333, and 353 K. Three-load creep tests were carried out at each temperature for of the wire samples to alloys. The deformation behavior and grain growth mechanism were investigated by strain-time curve analysis and microstructure observations. The results obtained show that the general characteristics of strain-time curve and microstructure of Sn-5wt% Sb alloy sensitively depend on the deformation temperature and strain rate. New free grains have been nucleated in microstructures in the process of dynamic recrystallization. These grains grow during deformation, forming coarser structure and elongation. The dynamic recrystallization and grain growth increase with increasing deformation temperature and decreasing strain rate. From the steady state creep rate the stress exponent is described in terms of the heat treatment temperatures. The stress exponent (n) were determined to clarify the deformation mechanism. Based on the n values, it is suggested that the rate controlling creep-deformation mechanism is dislocation climb. This study revealed that the solder alloy Sn–5wt%Sb have potential to give a good combination of higher creep resistance and rupture time.
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变形对Sn-5wt%Sb合金力学性能的影响
Sn-5wt %Sb是电子封装中考虑替代含铅合金的材料之一。研究了Sn-5wt % Sb钎料合金在不同应变速率和三种变形温度下的力学响应。研究了Sn-5wt % Sb钎料合金在313、333和353 K的应变速率和变形温度下的真应变时间行为。在不同温度下,对钢丝试样进行了三载荷蠕变试验。通过应变-时间曲线分析和显微组织观察,研究了复合材料的变形行为和晶粒长大机理。结果表明,变形温度和应变速率对Sn-5wt% Sb合金的应变-时间曲线和显微组织有敏感的影响。在动态再结晶过程中,在显微组织中形成了新的自由晶粒。这些晶粒在变形过程中长大,形成较粗的组织和伸长率。动态再结晶和晶粒长大随变形温度的升高和应变速率的降低而增大。从稳态蠕变速率出发,用热处理温度来描述应力指数。通过测定应力指数(n)来阐明变形机理。根据n值,提出了位错爬升控制蠕变速率的机制。研究表明,Sn-5wt %Sb钎料合金具有较高的抗蠕变性能和较长的断裂时间。
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