Fracture properties and mechanisms for irradiated austenitic steels over high temperature range and formulation of fracture criterion. Part 1. Experimental results

B. Margolin, A. Sorokin, A. Buchatsky, V. A. Shvetsova, O. Prokoshev, N. Pirogova
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Abstract

The experimental study results of the fracture properties and mechanisms are represented over temperature range from 200 up to 600°С for austenitic 304 steel (18Cr–9Ni steel) in the following conditions: (1) after neutron irradiation at temperature of 400°С up to damage dose of 30 dpa; (2) after neutron irradiation and subsequent aging at 550°С for 3000 hours. The fracture properties and mechanisms are determined under uniaxial tension of standard smooth cylindrical specimens and notched cylindrical specimens, i.e. for various stress triaxialities. Sharp decrease in the fracture strain and transition to intergranular fracture are revealed over high temperature range forstandard smooth cylindrical specimens. Over the same temperature range the fracture strain is larger for notched cylindrical specimens than for smooth cylindrical specimens, moreover a portion of intergranular fracture is also larger. This finding is rather abnormal as the fracture strain usually decreases when stress triaxiality and intergranular fracture portion increase. The obtained results are used for formulation of fracture criterion and elaboration of fracture model for high temperature radiation embrittlement that is considered in the second part of the paper.
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辐照奥氏体钢高温断裂性能和机理及断裂准则的制定。第1部分。实验结果
对304奥氏体钢(18Cr-9Ni钢)在200 ~ 600°С温度范围内的断裂性能和断裂机制进行了实验研究:(1)在400°С中子辐照至30 dpa损伤剂量后;(2)中子辐照后,在550°С老化3000小时。测定了标准光滑圆柱形试样和缺口圆柱形试样在单轴拉伸下的断裂性能和断裂机制,即不同应力三轴性下的断裂性能。在高温范围内,标准光滑圆柱形试样的断裂应变急剧下降,并向晶间断裂过渡。在相同温度范围内,有缺口柱状试样的断裂应变大于光滑柱状试样,且部分沿晶断裂也较大。这一发现是相当不正常的,因为断裂应变通常随着应力三轴性和晶间断裂部分的增加而减小。所得结果用于本文第二部分考虑的高温辐射脆化断裂准则的制定和断裂模型的阐述。
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