Extraction and Characterization of Fibres from the Stalk and Spikelets of Empty Fruit Bunch

Y. R. Nafu, Y. R. Nafu, J. Foba-Tendo, E. Njeugna, G. Oliver, Kavian Omar Cooke
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引用次数: 27

Abstract

Fibres from different parts of empty fruit bunch, which is a major solid waste from oil palm processing, were subjected to different pretreatments and characterised for variability in length and diameter, mechanical performance, and proximate and trace element composition. Morphology and surface composition of the fibres were determined using scanning electron microscopy with energy dispersive X-ray. The fibres were further treated with KOH-boric acid and characterized by Fourier transform infrared spectroscopy, X-ray diffraction, and scanning electron microscopy. Fibre yield was higher for spikelet than stalk. Fibres from stalk were generally larger in diameter and showed significant differences in potassium and galacturonic acid content, strength, and rigidity. Scanning electron microscopy confirmed the widespread occurrence of silica bodies as well as significant differences in the microstructure of stalk and spikelet fibres. Stalk fibres showed a greater level of porosity than spikelet fibres in the section perpendicular to the major axis. The morphology of KOH-boric acid treated fibres suggested higher recalcitrance of spikelet fibres. The significant differences between fibres from stalk and spikelet suggest that EFB, used as feedstock for biobased industries, requires more systematic characterization and separation into stalk and spikelet, which may lead to a more judicious exploitation of this valuable waste.
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空果串茎、小穗纤维的提取及特性研究
空果束是油棕加工过程中的主要固体废物,其不同部分的纤维经过不同的预处理,其长度和直径、机械性能以及近似和微量元素组成的变化都具有不同的特征。利用能量色散x射线扫描电子显微镜测定了纤维的形态和表面组成。用koh -硼酸对纤维进行进一步处理,并用傅里叶变换红外光谱、x射线衍射和扫描电镜对纤维进行表征。小穗的纤维产量高于茎。茎秆纤维一般直径较大,钾和半乳糖醛酸含量、强度和刚性差异显著。扫描电镜证实了硅体的广泛存在以及茎和穗纤维微观结构的显著差异。茎秆纤维在垂直于长轴的部分比小穗纤维表现出更大的孔隙度。氢氧化钾硼酸处理后的纤维形态表明,小穗纤维具有较高的抗逆性。来自秸秆和小穗的纤维之间的显著差异表明,作为生物基工业原料的EFB需要更系统的表征和分离成秸秆和小穗,这可能导致更明智地利用这种有价值的废物。
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