Synthesis and Characterization of Ternary Composite g-C3N4-MoO3/rGO for Photocatalytic Activity

Zain Waheed, Sadia Ghazanfar, M. Usman, Kalid Mahmood, Ajaz Hussain, Muhammad Siraj Ud din, Muhammad Tariq
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引用次数: 1

Abstract

The present research prepared a ternary composite g-C3N4-MoO3/rGO using the ultrasonic-assisted wet impregnation method. The prepared photocatalyst was characterized by using Fourier transform infrared spectroscopy (FT-IR), Powder X-ray diffraction (XRD), scanning electron microscopy (SEM), and EDX(Energy dispersive X-ray) techniques.  The structure and morphology of pure MoO3, g-C3N4, binary composite g-C3N4-MoO3, and ternary composite g-C3N4-MoO3/rGO have been studied in their photocatalytic performance in the degradation of  Rhodamine B (Rh-B) was tested and compared. The ternary composite g-C3N4-MoO3/rGO exhibited better degradation efficiency of 80% than pure and binary composite. The synergistic effect of the three components resulted in enhanced light-capturing ability, high charge separation, and low recombination rate of electron-hole pair. 

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g-C3N4-MoO3/rGO三元复合材料光催化活性的合成与表征
本研究采用超声辅助湿浸渍法制备了g-C3N4-MoO3/rGO三元复合材料。采用傅里叶变换红外光谱(FT-IR)、粉末x射线衍射(XRD)、扫描电镜(SEM)和能量色散x射线(EDX)技术对所制备的光催化剂进行了表征。研究了纯MoO3、g-C3N4、二元复合材料g-C3N4-MoO3和三元复合材料g-C3N4-MoO3/rGO的结构和形貌,并对其光催化降解罗丹明B (Rh-B)的性能进行了测试和比较。三元复合材料g-C3N4-MoO3/rGO的降解效率为80%,优于纯复合材料和二元复合材料。三种组分的协同作用增强了光捕获能力,提高了电荷分离率,降低了电子-空穴对的复合率。
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